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Synthesis of propanamide
For method number 3 I would have bubbled dry ammonia into the propanoyl bromide from an ammonia gene ...		 18-4-2016 at 15:09
by: Alkoxide
Al/NiCl2*6H2O: OTC hydride-like reactivity
That definitely looks useful! No exotic chems needed and it has good yields for a wide variety of re ...		 13-4-2016 at 03:52
by: Alkoxide
Potassium Iodide
I bought powdered caffeine from them a few years ago without an issue. I don't believe there are any ...		 11-4-2016 at 10:55
by: Alkoxide
is this a good vacuum pump?
You can definitely find some good deals on ebay. I bought a KNF 2 stage vacuum pump with PTFE heads ...		 9-4-2016 at 05:45
by: Alkoxide
government restrictions why bother
Many politicians are a special kind of special. They pass these laws for public appeal so they can g ...		 5-4-2016 at 07:48
by: Alkoxide
Simple(er)Aluminum Isopropoxide prep experiment for later this week.
I was able to repeat scientician's synthesis using gallium as a catalyst.

Procedure:

250mL of ...		 1-4-2016 at 04:31
by: Alkoxide
When Chemistry Goes Wrong
My biggest mishap came in organic lab I two years ago. I don't remember what the lab was, but I do r ...		 29-3-2016 at 20:56
by: Alkoxide
Pyridine via CuCl2 catalyzed decarboxylation
This afternoon I attempted to decarboxylate nicotinic acid (niacin) via CuCl2 to produce pyridine. T ...		 11-10-2015 at 13:21
by: Alkoxide
Bad days in the lab or with glassware?
Two weekends ago I attempted my first vacuum distillation. I had refluxed isopropanol with calcium o ...		 8-10-2015 at 05:45
by: Alkoxide
Preparation of solid aluminium isopropoxide
I haven't read it, I don't have access. Panziandi made Al(i-PrO)3 with iodine instead of mercury chl ...		 13-5-2015 at 20:47
by: Alkoxide
Preparation of solid aluminium isopropoxide
When you put it in terms of molar percent, the amount of water present seems much more significant. ...		 13-5-2015 at 15:12
by: Alkoxide
Preparation of solid aluminium isopropoxide
The isopropanol is supposed to be 99%. I wasn't sure if 1% water would have an effect on the reactio ...		 13-5-2015 at 14:55
by: Alkoxide
Preparation of solid aluminium isopropoxide
[rquote=404835&tid=12831&author=byko3y]In your case, iodine generates some amount of isoprop ...		 13-5-2015 at 14:33
by: Alkoxide
Aluminum Isopropoxide issues
Today was my first attempt at synthesizing aluminum isopropoxide. The reaction didn't go as planned. ...		 13-5-2015 at 12:30
by: Alkoxide

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