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Preparation of n-butylamine(consult)
So after about 40 hours at ~60-65C(with s.stirring) - almost none of my n-chlorobutane converted to ...
7-10-2020 at 04:41
by: B.D.E
Preparation of n-butylamine(consult)
Thanks for all the ideas and information! It really expanded my mind and knowledge on the matter, wh ...
26-9-2020 at 02:48
by: B.D.E
Preparation of n-butylamine(consult)
[rquote=645044&tid=156202&author=stoichiometric_steve][rquote=645041&tid=156202&auth ...
23-9-2020 at 04:08
by: B.D.E
Preparation of n-butylamine(consult)
Hey there, I'm in need for some n-butylamine and I would highly appreciate your consult and advice r ...
23-9-2020 at 00:33
by: B.D.E
Lead 2 acetate basic
[rquote=644626&tid=156161&author=dextro88]
and find out the tryhidrate is just with 3 OH ca ...
16-9-2020 at 05:23
by: B.D.E
Lead 2 acetate basic
[rquote=644626&tid=156161&author=dextro88]
but that mean i will need atlest some water in t ...
16-9-2020 at 05:17
by: B.D.E
Steven's Rearrangement - Alternative strong bases to NaNH2
First let me just say that Thomas Thompson is a [b][i]bitching name[/i][/b].

Second, although I w ...
27-8-2020 at 00:58
by: B.D.E
Synthesis, storage of sodium ethoxide
[rquote=643507&tid=156007&author=unionised][rquote=643501&tid=156007&author=S.C. Wac ...
25-8-2020 at 21:30
by: B.D.E
Synthesis, storage of sodium ethoxide
Just saying that producing sodium is quite fun as well.
Also, lithium is quite cheap(per mole) on e ...
21-8-2020 at 06:35
by: B.D.E
Synthesis, storage of sodium ethoxide
Never tried the method you've decscribed, but I have made some sodium alkoxides in the past by addin ...
12-8-2020 at 08:36
by: B.D.E
HotPlate Branding
[rquote=640599&tid=155794&author=Deathunter88][rquote=640598&tid=155794&author=Brigh ...
19-7-2020 at 21:53
by: B.D.E
KCN synthesis. Care to share your thoughts?
[rquote=640571&tid=155774&author=SWIM]
@B.D.E. I just realized that your post was the first ...
14-7-2020 at 12:35
by: B.D.E
KCN synthesis. Care to share your thoughts?
Using a cold diluted NaOCl+NaOH solution for the bubbler is probably good enough choice. Keep in min ...
12-7-2020 at 01:15
by: B.D.E
successful method for purifying anthranilic acid(quick report)
[rquote=640141&tid=155744&author=mackolol]In case of anthranillic acid, I don't see any othe ...
8-7-2020 at 12:54
by: B.D.E
successful method for purifying anthranilic acid(quick report)
[rquote=640138&tid=155744&author=mackolol]...[/rquote]
Glad to hear you find it useful :)
...
8-7-2020 at 08:06
by: B.D.E
successful method for purifying anthranilic acid(quick report)
[rquote=640125&tid=155744&author=Tsjerk]Why would higher boiling alkanes work faster? The ac ...
8-7-2020 at 05:36
by: B.D.E
does autoignition temperature even matter when refluxing a liquid?,
Ace :cool:
Thanks for the useful answers!
7-7-2020 at 11:47
by: B.D.E
successful method for purifying anthranilic acid(quick report)
Hey, this is a quick report on a successful attempt of mine to purify anthranilic acid made from pht ...
7-7-2020 at 10:49
by: B.D.E
does autoignition temperature even matter when refluxing a liquid?,
I mean, the max temprature probably going to be very close to the b.p, isn't it?

I'm asking becau ...
6-7-2020 at 03:36
by: B.D.E
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=639152&tid=155581&author=Boffis]OK here's a translation of the most useful paper fro ...
30-6-2020 at 01:03
by: B.D.E
Forbidden Knowledge!
[rquote=639083&tid=155647&author=Refinery]...[/rquote]
True. Although most of the times' th ...
24-6-2020 at 11:19
by: B.D.E
Forbidden Knowledge!
[rquote=639034&tid=155647&author=dawt]...[/rquote]
+They always use those impractical 0.1mm ...
23-6-2020 at 23:49
by: B.D.E
Forbidden Knowledge!
For the most, this "forbidden chemistry" you're talking about is just mundane chemistry employed ont ...
23-6-2020 at 07:20
by: B.D.E
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
@Tsjerk Great write-up man. I must admit it's a bit disappointing to hear that even though you seeme ...
23-6-2020 at 06:25
by: B.D.E
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=638817&tid=155581&author=Boffis]...[/rquote]
As for the solid that formed after add ...
20-6-2020 at 04:53
by: B.D.E
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