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1,4-Dioxane from Ethylene Glycol and H2SO4
[rquote=691182&tid=65311&author=Sir_Gawain]I was distilling dioxane over sodium metal once a ...
27-2-2024 at 14:50
by: Chemateur80
How do I recrystallize ferric chloride?
[rquote=691181&tid=83221&author=Texium]It actually doesn’t matter. It’s a bit difficult ...
27-2-2024 at 14:40
by: Chemateur80
1,4-Dioxane from Ethylene Glycol and H2SO4
I had an interesting experience some years ago when distilling 1,4-dioxane from Na-Mg-aggregate to d ...
26-2-2024 at 09:23
by: Chemateur80
How do I recrystallize ferric chloride?
[rquote=691116&tid=83221&author=clearly_not_atara]The easiest thing to do is to titrate the ...
26-2-2024 at 08:44
by: Chemateur80
How do I recrystallize ferric chloride?
This is a bit off topic, but since I'm going to use my ferric chloride to try to make ferric ammoniu ...
22-2-2024 at 13:15
by: Chemateur80
How do I recrystallize ferric chloride?
Thanks for the suggestions. There seems to be a few threads here about ferric ammonium sulfate, but ...
22-2-2024 at 13:00
by: Chemateur80
How do I recrystallize ferric chloride?
This looks like a good thread to bump when one’s interested in making some solid iron chloride.
E ...
21-2-2024 at 13:45
by: Chemateur80
Potassium oxalate, K2C2O4
I couldn't find a thread about this substance, so here it is.

Attempted to synthesize this by mix ...
9-9-2019 at 09:14
by: Chemateur80
Silver Nitrate Synthesis
[rquote=504148&tid=25328&author=MrHomeScientist]Thanks! Glad you liked the videos. It's a ve ...
9-4-2018 at 05:39
by: Chemateur80
1,4-Dioxane from Ethylene Glycol and H2SO4
Thanks for your input greenlight and Vosoryx. Very interesting.
I will definitely use a larger flas ...
9-4-2018 at 05:13
by: Chemateur80
1,4-Dioxane from Ethylene Glycol and H2SO4
A little DCM worked very well for cleaning the magnets. Thanks for the tip Vosoryx.

So I'm kind o ...
4-4-2018 at 13:14
by: Chemateur80
1,4-Dioxane from Ethylene Glycol and H2SO4
I had a go at this synthesis. For now I plan to use the dioxane to extract sodium metal Nurdrage sty ...
23-3-2018 at 11:43
by: Chemateur80
Question: Red phosphorus purification
[rquote=505838&tid=10926&author=woelen]Red phosphorus is odorless, but in practice, samples ...
3-2-2018 at 14:23
by: Chemateur80
Question: Red phosphorus purification
[rquote=505803&tid=10926&author=LearnedAmateur]Phosphorus is apparently described to have th ...
3-2-2018 at 11:16
by: Chemateur80
Question: Red phosphorus purification
Greetings.

I decided to clean some of my red phosphorus a little.
It's been standing for a few y ...
3-2-2018 at 06:05
by: Chemateur80
Silver Nitrate Synthesis
[rquote=504141&tid=25328&author=MrHomeScientist]It's possible the particles you observed are ...
18-1-2018 at 09:54
by: Chemateur80
Silver Nitrate Synthesis
Yesterday I dissolved 1g of my silver nitrate in a small amount of HNO[sub]3[/sub]/dH[sub]2[/sub]O. ...
18-1-2018 at 07:43
by: Chemateur80
Silver Nitrate Synthesis
[rquote=504049&tid=25328&author=clearly_not_atara]I might be able to answer you if you can e ...
18-1-2018 at 07:30
by: Chemateur80
Silver Nitrate Synthesis
[rquote=503936&tid=25328&author=clearly_not_atara]I do not know the specifics of the HCl/H2O ...
16-1-2018 at 06:43
by: Chemateur80
Silver Nitrate Synthesis
[rquote=503580&tid=25328&author=clearly_not_atara]Hydrogen peroxide will oxidize both silver ...
15-1-2018 at 08:30
by: Chemateur80
Silver Nitrate Synthesis
How about washing the silver with a mix of HCl and H[sub]2[/sub]O[sub]2[/sub]?
Will it help to get ...
12-1-2018 at 08:46
by: Chemateur80
Silver Nitrate Synthesis
[rquote=503474&tid=25328&author=diddi]If you redisolve your Ag in Nitric, it will be obvious ...
12-1-2018 at 08:42
by: Chemateur80
Silver Nitrate Synthesis
I decided to precipitate the Ag with Cu.
Cu-wire was cleaned with distilled water and acetone, and ...
11-1-2018 at 08:06
by: Chemateur80
Silver Nitrate Synthesis
I have also seen a video by Chemplayer on Youtube where they dissolve AgCl in aqueous ammonia, creat ...
17-12-2017 at 11:41
by: Chemateur80
Silver Nitrate Synthesis
[rquote=500566&tid=25328&author=clearly_not_atara]Chemateur: from your link:

[quote]Silve ...
16-12-2017 at 06:26
by: Chemateur80
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