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How to find out, which of 2 products are more likely to form?
Could I solve this problem, if I turn the halogen with NaOH to an alcohol and attach a protective gr ... |
2-5-2018 at 03:28
by: DIBALL |
Failed synthesis of cyclohexanol from cyclohexene.
Maybe not a "clean" suggestion, but couldn´t you react it with some halogen like Br2 in an aqueous ... |
1-5-2018 at 12:40
by: DIBALL |
How to find out, which of 2 products are more likely to form?
Thanks!
Sadly this isn´t what I was hoping for... I want to do a gringard reaction with the imine, ... |
1-5-2018 at 12:37
by: DIBALL |
Grignard vs. organolithium
I did both reactions and for the organolithium reaction I just used elemental Lithium, which was sto ... |
1-5-2018 at 11:34
by: DIBALL |
How to find out, which of 2 products are more likely to form?
So if I have a reaction, where 2 products can be formed and only 1mol of the reactant is given to 1m ... |
1-5-2018 at 11:07
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
Good news everyone!
I had 2 productive days and a lot new and interesting was witnessed!
So I tr ... |
30-4-2018 at 17:38
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
[rquote=514906&tid=81256&author=Melgar]I mentioned using DMSO + spearmint as a catalyst once ... |
22-4-2018 at 12:57
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
[rquote=514629&tid=81256&author=Pumukli]In Scr0t's pirrolidine synthesis there is a lot of t ... |
17-4-2018 at 13:50
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
So, I have some updates and some things that I can´t figure out, so I hope you can help me.
A we ... |
17-4-2018 at 06:53
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
[rquote=512319&tid=81256&author=zed]
Copper Chromite might be a good catalyst. Seems to do ... |
30-3-2018 at 06:59
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
I tried to determine the melting point and some of it decomposed like Ammonium Chloride, so like Pum ... |
28-3-2018 at 16:06
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
Great job and pictures Pumukli! That brings us a good step closer!
I retried this a couple days a ... |
22-3-2018 at 15:39
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
I just remembered, that Ammonium chloride is poorly soluble in ethanol, but Methylamine HCl is solub ... |
16-3-2018 at 12:40
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
[rquote=510821&tid=81256&author=Boffis]@ Diball; when you heat glycine with glycols you get ... |
15-3-2018 at 13:57
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
Just mixed NaOH and Glycine in a test tube and after heating there was a reaction that released some ... |
15-3-2018 at 12:58
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
[rquote=510783&tid=81256&author=Chemi Pharma][
No absolutely water sensitive, cause the sub ... |
15-3-2018 at 11:38
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
[rquote=510777&tid=81256&author=LearnedAmateur]What was your exact procedure, starting from ... |
15-3-2018 at 11:00
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
I used way to much of PG. If think it was around 20-30mL. But since it has such a characteristic sme ... |
15-3-2018 at 10:32
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
As far as I know, the solvent is there to archive high temperatures and Propylenglycol has a BP of 1 ... |
15-3-2018 at 10:12
by: DIBALL |
Decarboxylation of Glycine to Methylamine?!
Well in theory it should be possible, or not?
I tried it with 1g of Glycine in Propylenglycol (no ... |
15-3-2018 at 09:32
by: DIBALL |
Schiffs base / imine with an amine salt?
Right now I´m trying to make a Schiffs base from a ketone with methylamine. And I wanted to know, i ... |
2-1-2018 at 10:12
by: DIBALL |
Diethyl Ether from Denatured alcohol?
Okay I just found the safety sheet and it says that it contains 3 things: ethanol, MEK and water.
... |
22-4-2017 at 17:05
by: DIBALL |
Diethyl Ether from Denatured alcohol?
Is there an easy way to find out, if my product contains methanol? On the bottle is only written, th ... |
22-4-2017 at 13:41
by: DIBALL |
Diethyl Ether from Denatured alcohol?
Since pure ethanol is quite expensive and denatured alcohol is only 1/10th of the price, I wanted to ... |
22-4-2017 at 13:02
by: DIBALL |
Is inert gas mandatory for handling DIBAL?
I want to perform a reduction with Diisobutylaluminium hydride (DIBAL), where 1mol of it is solved i ... |
4-1-2017 at 16:00
by: DIBALL |
