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2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
Like i wrote, no blaming, and no acusing - it wasn't directed at you, but at whoever might be readin ... |
19-12-2008 at 20:35
by: Dextrose |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
Yeah, science instead of point-less discussions.
Anyhow, i will point out that if you read "2,5-d ... |
19-12-2008 at 18:49
by: Dextrose |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
I don't get this... Are someone being flamed here, or did brew just had a bad day?
Where i am res ... |
19-12-2008 at 17:41
by: Dextrose |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
[quote][i]Originally posted by Isomeric_Fred[/i]
I spoke to niobium, who said that EDDA is ethylene ... |
18-12-2008 at 21:10
by: Dextrose |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
[quote][i]Originally posted by stoichiometric_steve[/i]
Dextrose, i wouldn't be too sure of that. M ... |
27-10-2008 at 21:36
by: Dextrose |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
Nice yield, but i have seen/heards reports of people getting 85-90+% in this condenzation using meth ... |
20-10-2008 at 08:39
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
[quote][i]Originally posted by Sandmeyer[/i]
How many times are you gonna attach the picture of sam ... |
16-10-2008 at 09:22
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Could it be more possible that a Reimer-Tiemann formylation of 2-methoxy-5-nitrophenol would yield t ... |
18-8-2008 at 14:24
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
[quote][i]Originally posted by Klute[/i]
I would rather go through the sulfonate, I'm pretty sure t ... |
11-8-2008 at 14:41
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Thank you once again, Ritter and Sonogashira...
I have been looking at nearly every indole synthe ... |
9-8-2008 at 18:43
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Yeah, i must admit that i also find the 3.rd the most plausible.
But 8 steps now, and it would be ... |
6-8-2008 at 16:50
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
...But if ethers or esters would direct the nitro-group correctly, like a sulfoxide, this would of c ... |
6-8-2008 at 13:34
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Here's the one i find most likely to work. |
6-8-2008 at 13:30
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Even though i'm pretty doubtfull myself, i'll post it anyway for flaming purporses. 
Would the ... |
6-8-2008 at 11:43
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Thank you for your replies, guys!
Ullmann, i haven't been able to find that paper, even the unive ... |
2-8-2008 at 04:41
by: Dextrose |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
I hope this topic will be taken more seriously.
I asked Shulgin about this compound 3 years ago, ... |
1-8-2008 at 07:30
by: Dextrose |
Lysergol oxidase?
If one hypothetically had a small amount of the clavine lysergol, which upon full oxidation would yi ... |
10-1-2008 at 10:16
by: Dextrose |
Chlorination of 2C-H using Sodium Hypochlorite (NaOCl)
Hello.
I have some 2C-H.HCl (2,5-dimethoxyphenethylamine.HCl) lying around waiting to get halogen ... |
25-10-2007 at 16:03
by: Dextrose |
Novel route to Methylone?
Thank you.
I must admit that AlCl3 as catalyst was just a wild guess, but i had no other ideas.
... |
13-1-2007 at 09:23
by: Dextrose |
Novel route to Methylone?
[quote][i]Originally posted by Nicodem[/i]
[quote][i]Originally posted by Dextrose[/i]
The questio ... |
13-1-2007 at 09:10
by: Dextrose |
Novel route to Methylone?
[quote]I know that propionyl chloride can be used in the first step, but i would really like to avoi ... |
13-1-2007 at 08:57
by: Dextrose |
Novel route to Methylone?
Hi there...
I've really set my mind on a Methylone synthesis, since all reagents and precursors a ... |
12-1-2007 at 21:37
by: Dextrose |
4-substituted-2,5-dimethoxyalkylamines
Sandmeyer, Nicodem > I'm sorry to piss you old hive-farts off (J/K). 
I hate off-topicness, ... |
8-11-2006 at 09:26
by: Dextrose |
2,5-DMPEA: hcl formation and preservation
[quote]Dextrose:
[quote]
Add 10x acetone, and suction-filter. Wash with additional acetone if ... |
8-11-2006 at 09:22
by: Dextrose |
P2NP microwave crystallization problem
Use another primary amine (salt), Methylamine.HCl should give kick-ass yields (Osmium).
AFOAF did ... |
4-11-2006 at 18:35
by: Dextrose |
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