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Chloroacetic acid from glycine or another bullshit patent?
Pity that trichlorethylene was banned already years ago, its hydrolysis gives very pure monochloroac ...
3-8-2020 at 14:01
by: Fery
mononitrophenols - nitration of phenol
Hi fdnjj6, be patient, I'll synthesize mononitrotoluenes soon (perhaps in 1 year at most) to synthes ...
30-7-2020 at 11:37
by: Fery
Recommendations for synthesis of medicines and other medical organic molecules.
If you are able to obtain lidocaine, you can synthesize denatonium from it, the most bitter substanc ...
30-7-2020 at 11:26
by: Fery
Recommendations for synthesis of medicines and other medical organic molecules.
Advanced Practical Medicinal Chemistry
https://www.pdfdrive.com/advanced-practical-medicinal-chemis ...
29-7-2020 at 04:27
by: Fery
1-bromo-2-ethylhexane normal pressure distillation?
https://www.sciencemadness.org/whisper/viewthread.php?tid=155698
distilled upto 224 C at normal pre ...
27-7-2020 at 22:08
by: Fery
1-bromo-2-ethylhexane normal pressure distillation?
https://www.lookchem.com/2-Ethylhexyl-bromide/
190,8 C at 760 mm Hg
27-7-2020 at 11:14
by: Fery
CsICl4 caesium tetrachloroiodate
Hi MadHatter, I was quite disappointed with the poor yield in May, so I let the mother liquor to eva ...
25-7-2020 at 22:32
by: Fery
mononitrophenols - nitration of phenol
The 8,5 g of dirtiest last crop of 4-nitrophenol was recrystalled this way:
3,0 g dissolved in 50 m ...
24-7-2020 at 11:39
by: Fery
CsICl4 caesium tetrachloroiodate
as the yield was even less than miserable, I let the mother liquor to evaporate at room temperature ...
24-7-2020 at 11:28
by: Fery
How to concentrate formic acid?
unionised is right, IIRC distillation at 0,2-0,3 atm produces 85% acid from 77% azeotrope which boil ...
24-7-2020 at 11:13
by: Fery
In case anyone's curious about acid burns, I spilled a small amount of boiling RFNA on my arm.
The reddish surrounding (barely visible for not trained eye) could be caused by an infection, but in ...
24-7-2020 at 11:09
by: Fery
Health effects of acute, low concentration acid vapors.
Airways are wet so traces of acid vapors are immediately neutralized with HCO3-. But higher concentr ...
24-7-2020 at 10:57
by: Fery
Procedure for Coumarin - different product, what is it?
I did not obtain that flat square-like crystals when recrystallizing from water. Too much water = co ...
21-7-2020 at 08:10
by: Fery
Procedure for Coumarin - different product, what is it?
Hi Pumukli, you are right, vanilla scent is only public shared info, real experience is better than ...
17-7-2020 at 03:54
by: Fery
How to recrystallize high solubility substances?
Do you want to recrystallize only inorganic substances? Sometimes you can use organic solvent. Or at ...
16-7-2020 at 07:14
by: Fery
In case anyone's curious about acid burns, I spilled a small amount of boiling RFNA on my arm.
Pls let us informed how it will evolve. The upper part of epidermis are just dead flat keratinocytes ...
16-7-2020 at 07:10
by: Fery
The Wump Incident
Fyndium - most of us were fascinated with pyro in our chemistry beginnings... I remember preparing " ...
16-7-2020 at 06:48
by: Fery
Most potent H2O2 decomposition catalysts available to an amateur
unionised - blood was my first idea too (as I often saw 3% medicinal H2O2 for cleaning wounds, bubbl ...
16-7-2020 at 06:17
by: Fery
Procedure for Coumarin - different product, what is it?
[b]Don't wash with NaOH[/b] as it splits the lactone ring. I'm currently performing the synthesis, j ...
16-7-2020 at 05:50
by: Fery
cinnamic acid
To 250 ml RBF (perhaps 100 ml is better, less air, less benzaldehyde oxidation to benzoic acid, on t ...
8-7-2020 at 04:12
by: Fery
cinnamic acid
I did the same synthesis as Magpie and Waffles SS, just without pyridine.
The catalyst base I used ...
8-7-2020 at 03:32
by: Fery
allyl valerate - pineapple ester
This is quite surprising for me, I found a pineapple scent sold in my country and most of its conten ...
6-7-2020 at 04:34
by: Fery
Reducing bumping in vacuum distillation
There is a big temperature difference on the surface of the vacuum distilled liquid - there is rapid ...
5-7-2020 at 10:01
by: Fery
Aesthetic Aromatics: Preliminaries
1,3,5-trinitrobenzene missing... TNT oxidation of -CH3 to -COOH using Na2Cr2O7+H2SO4 and then decarb ...
3-7-2020 at 11:23
by: Fery
heptyl butanoate - fruity and little of chamomile scent
Hi Tsjerk, you are right, that should help at the small cost that it won't be so well visible what h ...
1-7-2020 at 04:38
by: Fery
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