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Synthesis of Ethyl ß-Naphtholate (Nerolin) DraconicAcid great! Washing with KOH certainly got rid of unreacted naphthol. So you did a methylati ... |
4-12-2023 at 06:33 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 I did purity checks of the product by freezing it for half a year in fridge at +4 C, small oscillati ... |
4-12-2023 at 06:12 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 Do you mean the column attached to the reaction flask or do you mean the first distillation of the a ... |
3-12-2023 at 21:58 by: Fery |
Synthesis of 9,9‘-bianthracene from anthraquinone Niklas welcome here. Great experiment, beautiful fluorescence!!! |
3-12-2023 at 10:19 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 Hi Sir_Gawain, maybe the best route would be a continuous method like filling 500 ml RBF with 100 ml ... |
3-12-2023 at 09:52 by: Fery |
pseudoisomethylionone by Aldol condensation of citral with methylethylketone No way how to assess the purity.
I would like to perform a cyclization in 85% H3PO3 into alfa and ... |
29-11-2023 at 20:47 by: Fery |
pseudoisomethylionone by Aldol condensation of citral with methylethylketone dry crude product going to be predistilled at water aspirator pump vacuum level
[file]100116[/fi ... |
29-11-2023 at 11:19 by: Fery |
pseudoisomethylionone by Aldol condensation of citral with methylethylketone This experiment is a variation to this one, just a ketone with one more carbon was used and somethin ... |
29-11-2023 at 10:54 by: Fery |
Preparation of cyanogen bromide and a polymethine dye Good finding Diachrynic !!! More available route! Interesting that the Na2S2O8 gives that dimer by a ... |
29-11-2023 at 10:08 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 Everyone repeats the mistakes of former home lab experimenters although everyone sees the consequenc ... |
28-11-2023 at 21:40 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 [rquote=688970&tid=160001&author=Sir_Gawain]300 mL antifreeze, 30 mL sulfuric acid, 500 mL f ... |
28-11-2023 at 11:11 by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4 what was your ratio of ethylene glycol : H2SO4
volume of your flask and volume of reactants? |
28-11-2023 at 01:15 by: Fery |
pseudoionone by Aldol condensation of citral with acetone apparatus and the start of the reaction
[file]100018[/file]
the start of the reaction vis ... |
27-11-2023 at 11:13 by: Fery |
pseudoionone by Aldol condensation of citral with acetone wow the thread id is 160000
OK photos.
Distillation of citral
[file]100008[/file] [file]100010 ... |
27-11-2023 at 10:58 by: Fery |
pseudoionone by Aldol condensation of citral with acetone Various methods could be used, different ratio of reactants (ratio of excess of acetone), catalysts ... |
27-11-2023 at 10:56 by: Fery |
Contaminated 1-indanone sample It has quite low melting point so it oils out during recrystallization especially if the solvent is ... |
22-11-2023 at 08:20 by: Fery |
Persulfate oxidation? Permanganate [rquote=688563&tid=159963&author=RU_KLO]to check (test) persulfate as oxidizer[/rquote]
Add ... |
14-11-2023 at 21:06 by: Fery |
Disinfection of rainwater Alternatives like solar distillation or passing tap water through ion exchange resins (making deioni ... |
4-11-2023 at 04:56 by: Fery |
Mystery Glassware Identification Thread Also could be used as a fermentation tube.
https://sklep-chemland.pl/en/lejek-fermentacyjny.html |
2-11-2023 at 19:17 by: Fery |
Caffeine (>99% FG) for sale - 1kg If the caffeine was listed as food grade for consumption by humans then maybe some authorities force ... |
1-11-2023 at 21:18 by: Fery |
Glyoxal Synthesis Well done BAV Chem! For some reactions you can use directly the adduct of glyoxal with bisulfite lik ... |
1-11-2023 at 08:39 by: Fery |
Pretty Pictures (2) By the pyridine cheaply.
https://shop.es-drei.de/heterocyclen/163/pyridin-min.-99-5-zur-analyse
ht ... |
15-10-2023 at 19:01 by: Fery |
Pretty Pictures (2) [rquote=687945&tid=26378&author=andyloris]@Pumukli, where did you find your procedure for th ... |
14-10-2023 at 12:24 by: Fery |
Warfarin syntheses This seems to be a suitable home lab way for warfarin. But only racemic product. For obtaining stere ... |
10-10-2023 at 06:27 by: Fery |
Nitrous acid scavenger Aha, the HNO2 catalyzes nitration of some aromatic which I cannot remember from my head. For the alc ... |
5-10-2023 at 09:39 by: Fery |
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