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Formic acid from Hexamine/HCl? Fantastic work Anglehair!
I tried your last 25L synth and my results are on par with yours. Easi ... |
13-1-2014 at 19:26 by: FriendlyFinger |
Products from Ca benzoate and Ca propionate Besides P1P, what do you think are all the possible products from a dry distillation of Ca Benzoate ... |
2-12-2009 at 18:37 by: FriendlyFinger |
Sodium sulfite method for formaldehyde Can anybody please show me where I can find details on how to determine formadehyde concentration in ... |
17-12-2007 at 21:57 by: FriendlyFinger |
EtOH distillation EtOH distillation.
If you have a 50% water/Etoh mix and distill, will it come over at the same t ... |
17-12-2007 at 20:40 by: FriendlyFinger |
Method for MeNH2 detection On the Hive, I remember a thread where someone suggested separating NH4Cl from MeNH2.HCL by attachin ... |
17-12-2007 at 20:36 by: FriendlyFinger |
colour of Methylamine When making MeNH2.HCl from hexamine and HCl, after the reaction;
1) is the solution always yellow ... |
11-9-2006 at 23:58 by: FriendlyFinger |
question about distilling water I have a water distiller with nickel plated elements. I charge it up with tap water filtered through ... |
25-7-2006 at 19:33 by: FriendlyFinger |
Q. about hydrolyzing hexamine I was reading one of Festers books when I came across his directions for hydrolyzing hexamine, he su ... |
30-6-2006 at 18:45 by: FriendlyFinger |
Mantle or oil bath temp question. If I wanted to heat a temp sensitive solution to say 104 deg C, usually I would use an oil bath at a ... |
30-6-2006 at 18:36 by: FriendlyFinger |
titrating MeNH2 in methanol The other day I tried to titrate suspected 6% MeNH2 in MeOH, so I prepared 25 ml HCl containing 0 ... |
27-6-2006 at 23:43 by: FriendlyFinger |
"dry" acetone 7) What's the story with molecular sieves and acetone?
"Purification of laboratory chemicals" 5th ... |
27-6-2006 at 23:37 by: FriendlyFinger |
Benzene, toluene distillation speed? I'm using them to extract a temp sensitive compound and want to choose the faster distilling solvent ... |
7-6-2006 at 00:56 by: FriendlyFinger |
IPA extraction question If a had a block of a fairly anhydrous mix of MeHN2/NH4HCl, from a hexamine/HCl reaction and extract ... |
6-6-2006 at 01:56 by: FriendlyFinger |
Benzene, toluene distillation speed? What distills faster under vacuum, benzene or toluene? |
6-6-2006 at 01:49 by: FriendlyFinger |
40% aqueous MeNH2.HCl question Well thanks for that and yes it does make me feel better, I'll get up off the floor and do it again. ... |
2-6-2006 at 16:53 by: FriendlyFinger |
MeNH2.HCl via EtOH. How man !!! I believe I have reached the point of total madness with this easy synth that I have attempted 19 ti ... |
1-6-2006 at 01:28 by: FriendlyFinger |
40% aqueous MeNH2.HCl question What's the right way to prepare 40% aqueous methylamine solution?
In Festers SOMM he says, mix 1 ... |
1-6-2006 at 00:56 by: FriendlyFinger |
Thermal Decarboxylation - Alkyl Phenyl Ketones Oh! How do you do that? I know nothing about electrolytic cells. How much current? what medium do yo ... |
26-5-2006 at 02:26 by: FriendlyFinger |
Thermal Decarboxylation - Alkyl Phenyl Ketones What's the chance of this reaction working with ordinary non reduced iron powder? |
16-5-2006 at 02:33 by: FriendlyFinger |
Thermal Decarboxylation - Alkyl Phenyl Ketones Well blow me down. Solo, please mail me your shoes, I keep them under my bed!
Thank you very much |
2-5-2006 at 20:52 by: FriendlyFinger |
Thermal Decarboxylation - Alkyl Phenyl Ketones Could someone please post another link or at least the name of these two articles so I can look for ... |
29-4-2006 at 19:24 by: FriendlyFinger |
Performic & P2P. Experiments & observations Swim wrote;
" It was hoped that the modern buffered Performic would do for propenylbenzene that ... |
23-4-2006 at 19:29 by: FriendlyFinger |
Propenylbenzene synth. Comments and suggestions please Example 1.
500g P1P (3.73 mole)
43g NaBH4 (1.14 mole)
1250ml MeOH
746ml dH2O
4.5 7g NaOH ... |
23-4-2006 at 19:17 by: FriendlyFinger |
Green methylamine Swim said
"the other day I was refluxing hexamine with a slight overdose of HCl forgetting about ... |
18-3-2006 at 19:19 by: FriendlyFinger |
"dry" acetone Then it says shake for a few hours with 25g/l CaSO4, decant and distill through a column with 10g/l ... |
18-3-2006 at 18:29 by: FriendlyFinger |
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