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Problem when trying to vacuum distil a compound.
I really appreciate both of your feedback, in future I will endeavour to word my questions in a way ... |
20-12-2025 at 14:10
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
[rquote=704837&tid=161431&author=jackchem2001]How is anybody supposed to help about a distil ... |
19-12-2025 at 23:20
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
Not entirely sure what a meyer schuster is, I have always known it as a Pinacol Rearangment.
And ... |
18-12-2025 at 16:22
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
Update: I did redistilled my product and the same issue reoccured. I turned up the stirring to maxim ... |
18-12-2025 at 14:58
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
[rquote=704673&tid=161431&author=bnull]My first question would be what organic liquid is it. ... |
18-12-2025 at 14:51
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
On that note, yes I have started to think it could have been residual DCM in my product boiling out, ... |
13-12-2025 at 18:11
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
Ok, so I performed the reaction on half the scale as the writeup, but used 15g of product instead of ... |
13-12-2025 at 18:07
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
[rquote=704652&tid=161431&author=fx-991ex][rquote=704650&tid=161431&author=Sulaiman] ... |
11-12-2025 at 14:51
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
No but I did use magnetic stirring, which I believe is a better option than boiling chips for vacuum ... |
11-12-2025 at 01:27
by: GhostAliensFromMars |
Problem when trying to vacuum distil a compound.
I was attempting to purify an organic liquid I synthesised at my university using fractional distill ... |
11-12-2025 at 00:31
by: GhostAliensFromMars |
77.5% formic acid
Right I ran into a small problem during the distilation to get the 77.5% azeotrope
The acid was h ... |
22-10-2025 at 14:57
by: GhostAliensFromMars |
77.5% formic acid
Right I ran into a small problem during the distilation to get the 77.5% azeotrope
The acid was h ... |
22-10-2025 at 14:57
by: GhostAliensFromMars |
77.5% formic acid
"Distill your 65% acid to the azeotrope, add a lot of anhydrous copper sulfate to the distillate, le ... |
25-9-2025 at 23:47
by: GhostAliensFromMars |
77.5% formic acid
Alright, looks like I'm gonna have to try out the cuso4 drying. Quick question, if one had formic ac ... |
25-9-2025 at 00:22
by: GhostAliensFromMars |
77.5% formic acid
Hello
I have read through a number of threads regarding the drying of azeotropic formic acid to i ... |
24-9-2025 at 19:46
by: GhostAliensFromMars |
Separating a mixture containing solvents and a dissolved solid that sublimes
Hmm, thx for the ideas. Perhaps il just first stir the mixture with no heat and apply a vacuum to su ... |
30-4-2025 at 01:42
by: GhostAliensFromMars |
Separating a mixture containing solvents and a dissolved solid that sublimes
Its made up of about 50% camphor dissolved in around 20%eugenol and 20% cineole. According to the MS ... |
29-4-2025 at 22:38
by: GhostAliensFromMars |
Separating a mixture containing solvents and a dissolved solid that sublimes
Hi all
I have a small question regarding separation. If one had a mixture of different liquids co ... |
28-4-2025 at 23:01
by: GhostAliensFromMars |
Sassafras oil long term storage
Do you know of any other ways an amatuer could detect the prescene of the allylbenzene? I set up for ... |
3-4-2025 at 21:51
by: GhostAliensFromMars |
Sassafras oil long term storage
just tried this today, here's my results.
In my front yard is a relatively large camphor tree. ... |
2-4-2025 at 20:48
by: GhostAliensFromMars |
Sassafras oil long term storage
could I just instead perform a solvent extract of the camphor wood with ethanol, and fractionally di ... |
1-4-2025 at 21:02
by: GhostAliensFromMars |
Demethylation of Eugenol
"Imoto and Ono, Journal of the Chemical Society of Japan, vol 55, pg 275-9 (1934) (Chemical Abstract ... |
11-12-2024 at 00:53
by: GhostAliensFromMars |
Demethylation of Eugenol
The link contains lots of different demethylation methods, perhaps the most interesting one is the ... |
4-12-2024 at 21:15
by: GhostAliensFromMars |
Sassafras oil long term storage
Would you know if using toluene instead of acrylonitrile as the solvent will work? Acrylonitrile is ... |
27-11-2024 at 02:56
by: GhostAliensFromMars |
Sassafras oil long term storage
Thanks for the resources, correct me if im wrong but is this process: (https://www.youtube.com/watch ... |
18-11-2024 at 15:20
by: GhostAliensFromMars |
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