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aldehyde to amide musings and needed help
I am unsure to which compound S.C.Wack is hinting at. Thanks for your helpful participation anyway.
... |
20-6-2010 at 02:33
by: Isomeric_Fred |
aldehyde to amide musings and needed help
Hello fellow SM members.
Im on the lookout for a procedure that will convert an aldehyde to amide. ... |
19-6-2010 at 12:18
by: Isomeric_Fred |
Cinnamamide purification
Hi Klute. I havent carried out the reaction with acrylamide yet, since I wasnt sure about how to pur ... |
4-3-2009 at 13:15
by: Isomeric_Fred |
Cinnamamide purification
Hi Nicodem and thanks 
Yes I am carrying out heck couplings. celite aid filtration is a must here ... |
25-2-2009 at 04:34
by: Isomeric_Fred |
Cinnamamide purification
Hello. Long time no post, but I find myself in need of help and this is the natural place for me to ... |
25-2-2009 at 03:47
by: Isomeric_Fred |
Reductions of Nitro groups with Zn and acid
[quote][i]Originally posted by Barium[/i]
[quote][i]Originally posted by Isomeric_Fred[/i]
Perhaps ... |
29-10-2008 at 04:23
by: Isomeric_Fred |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
[quote][i]Originally posted by Nicodem[/i]
Please stop with this nonsense. "EDDA" in this case stan ... |
28-10-2008 at 05:19
by: Isomeric_Fred |
Reductions of Nitro groups with Zn and acid
[quote][i]Originally posted by Barium[/i]
[quote][i]Originally posted by stoichiometric_steve[/i]
... |
28-10-2008 at 00:42
by: Isomeric_Fred |
The CTH Writeup by Barium as Tried Out by Bandil. Sciencemadness Members Clear Things Up!
I have to support stoichiometric_steve on this. Man, did I cry multiple times when trying out some o ... |
28-10-2008 at 00:32
by: Isomeric_Fred |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
I spoke to niobium, who said that EDDA is ethylenediamine diacetic acid salt.
Dextrose, i highly d ... |
28-10-2008 at 00:28
by: Isomeric_Fred |
TCT (Cyanuric Chloride)
sorry to pull this up after such a long time, but the preperations you noted Sauron are not in the a ... |
17-7-2007 at 00:51
by: Isomeric_Fred |
N-Halosuccinimide Solvents Workaround ??
I have used NCS in DCM with success and no apperent solvent chlorination.
EDIT ::
Also I have use ... |
4-7-2007 at 15:32
by: Isomeric_Fred |
3-phenylpropan-1-ol chlorination
i havent looked solo, but cyanuric chloride might be good for your needs. AFAIK it is excellent in c ... |
4-7-2007 at 15:25
by: Isomeric_Fred |
Clemmensen reduction
you should look into ni/al alloy (not raney nickel, an alloy). not sure if they reduce halogens, but ... |
4-7-2007 at 15:23
by: Isomeric_Fred |
3-phenylbutan-2-one info needed
Hi.
Been searching for the physical data of 3-phenybutan-2-one but cant find any. Not on Merck, and ... |
4-7-2007 at 14:30
by: Isomeric_Fred |
Ketone to amine: in search of a greener way...
attached is a rar file with interesting refs about nabh4 and additive as reductive amination reagent ... |
8-2-2007 at 12:49
by: Isomeric_Fred |
Ketone to amine: in search of a greener way...
apperently sodium triacetoxy borohydride (prepared in-situ from sodium borohydride +3 acetic acid) i ... |
6-2-2007 at 13:39
by: Isomeric_Fred |
Extraction problems.
look Furch, you said -
"I have a problem. You see, I'm trying to perform a reductive amination wit ... |
21-1-2007 at 08:25
by: Isomeric_Fred |
Extraction problems.
we would like to contribute our 2 cents.
first of all, better to make reaction in ethanol in our ex ... |
20-1-2007 at 07:13
by: Isomeric_Fred |
new/old nitroalkene reduction method
here it is, as you requested. note that this is for azides, but alot can be learned from this regard ... |
11-12-2006 at 17:49
by: Isomeric_Fred |
NaBH4/CuSO4 nitro reduction success!!
update - still we have not got consistent results from cupric sulfate/sodium borohydride reduction. ... |
11-12-2006 at 04:23
by: Isomeric_Fred |
new/old nitroalkene reduction method
Dear sandmayer, in the topic it is named new/old, and in the post itself, it is said as "verificatio ... |
11-12-2006 at 04:21
by: Isomeric_Fred |
new/old nitroalkene reduction method
Dear sciencemadnessers,
We would like to share with you our latest findings as promised some time a ... |
10-12-2006 at 15:22
by: Isomeric_Fred |
NaBH4/CuSO4 nitro reduction success!!
the problem with nabh4/cth is that sometimes the nabh4/nitro form a complex nitronate which traps ni ... |
13-10-2006 at 01:59
by: Isomeric_Fred |
NaBH4/CuSO4 nitro reduction success!!
NaBH4/CuSO4 system in EtOH/H2O was given another shot.
phenylnitroalkane was reduced in reflux to y ... |
27-9-2006 at 22:15
by: Isomeric_Fred |
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