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Home Lab Construction
I am going to be pouring a foundation for a new home next week, and I want to have a home lab. I sti ...
4-8-2021 at 18:44
by: JJay
Chromium pentoxide uses
It's been far too long since I was on here....

Pyridine can be used to stabilize chromium VI oxid ...
3-8-2021 at 15:58
by: JJay
Nickel benzoate
[rquote=651782&tid=156781&author=RustyShackleford]I have tried thermal decomposition of calc ...
22-12-2020 at 13:01
by: JJay
Domestic (USA) sodium borohydride or lithium aluminum hydride?
[rquote=651788&tid=156778&author=thors.lab][rquote=651787&tid=156778&author=JJay]Sod ...
22-12-2020 at 10:34
by: JJay
Domestic (USA) sodium borohydride or lithium aluminum hydride?
Sodium borohydride is sometimes freely available in bulk and sometimes expensive and hard to find. L ...
21-12-2020 at 14:42
by: JJay
Latest chemical order?
I didn't place any new orders, but my adipic acid finally arrived. Also, my sodium borohydride final ...
28-11-2020 at 17:39
by: JJay
Nitriles and aldehydes from amino acids and bromosuccinimide
One major issue in these sorts of reactions is whether the amino acid is monohalogenated or dihaloge ...
28-11-2020 at 17:35
by: JJay
Latest chemical order?
I ordered some adipic acid. I want to try making some cubanes when I get a chance to do some chemist ...
1-10-2020 at 01:45
by: JJay
new toys
[rquote=644314&tid=64800&author=draculic acid69][rquote=488477&tid=64800&author=JJay ...
7-9-2020 at 21:03
by: JJay
Latest chemical order?
Sodium thiosulfate is good for neutralizing halogens. BHT is good for stabilizing ether. Sodium meta ...
31-8-2020 at 10:43
by: JJay
Fume Hood Construction
[rquote=643868&tid=67117&author=beta4]I started working last year with the idea of building ...
29-8-2020 at 21:24
by: JJay
Oxidation of styrene to phenylacetaldehyde
I would probably suggest the bisulfite adduct-forming procedure written by Eleusis as the easiest an ...
29-8-2020 at 20:49
by: JJay
How are highly hygroscopic things purified via recrystallization?
Umm... IDK much about GHB, but I think it's a fairly stupid drug - kind of like ethanol in terms of ...
29-8-2020 at 19:58
by: JJay
Small scale production of H2SO4 in the amateur lab
I'm not 100% sure if I'm going to be able to find and unpack everything I need to do a trial run of ...
27-8-2020 at 22:26
by: JJay
Nitric acid questions
If you do use a thermometer, it's a good idea to use a glass thermometer well - a rubber or plastic ...
26-8-2020 at 08:08
by: JJay
new toys
I got a 5 gallon vacuum chamber. The lid appears to be plexiglass. The vacuum gauge will actually me ...
25-8-2020 at 11:21
by: JJay
latest glassware purchase
I'll see what I can do. I don't actually have a purpose for it yet, but I'm sure I'll come up with o ...
25-8-2020 at 02:38
by: JJay
Latest chemical order?
Tribasic calcium phosphate
Sodium bromide
Tartaric acid
Tin (ingot)
Zinc oxide
3A molecular sei ...
24-8-2020 at 20:30
by: JJay
latest glassware purchase
I picked up an auger funnel, a backup 90mm 1L pore plate funnel (which is very high quality and ring ...
24-8-2020 at 20:05
by: JJay
Screens for Aluminum Powder
[rquote=643595&tid=156077&author=RogueRose]I'm in the process of building seives and a shake ...
24-8-2020 at 02:43
by: JJay
Screens for Aluminum Powder
I see quite a few laboratory sieve shakers on eBay. They're not cheap. I also see shakers that are a ...
23-8-2020 at 09:58
by: JJay
adjustable mini stove + additional questions
You probably don't want an ultralight stove for doing chemistry. When I need a flame, I typically us ...
23-8-2020 at 04:52
by: JJay
Chloroform from calcium hypochlorite
The part about purification with sulfuric acid seems to have been glossed over in many modern descri ...
22-8-2020 at 15:17
by: JJay
Screens for Aluminum Powder
I've been wanting to try out some exotic thermites. I have a small rock tumbler and some blenders th ...
22-8-2020 at 12:27
by: JJay
Tar from H2SO4 + sugar reaction?!
The carbon made from the reaction is called sugar carbon. I've read books that discuss it, and it's ...
22-8-2020 at 09:16
by: JJay
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