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double bond reduction of alpha-methylnitrostyrenes with NaBH4
[rquote=348347&tid=5436&author=Rabodon][rquote=347578&tid=5436&author=Templar]Wasn't ...
25-9-2014 at 22:14
by: JefferyH
99% IPA in store?
I checked a number of stores... zilch.

Decided to make my own.... stirring 4x excess anhydrous m ...
25-9-2014 at 22:07
by: JefferyH
Sugestions for a first EASY SAFE Vacuum distilation
You don't want solvents escaping through your vacuum, it can cause some problems in the vacuum. Also ...
25-9-2014 at 15:31
by: JefferyH
99% IPA in store?
What electronic stores did you get IPA from, and in what size bottles? Best Buy? RadioShack? Does it ...
25-9-2014 at 14:59
by: JefferyH
Diy copper Liebig condenser.
Laboratory distillation does not [i]have[/i] to be done with glassware, but if you are using somethi ...
20-9-2014 at 08:25
by: JefferyH
99% IPA in store?
[rquote=346777&tid=34384&author=forgottenpassword]How can a 1% impurity cause a lot of troub ...
20-9-2014 at 01:42
by: JefferyH
99% IPA in store?
I have heard on numerous occasions that this can be found in stores such as auto-supply places, but ...
20-9-2014 at 00:41
by: JefferyH
Washing a halogen contaminated aromatic aldehyde with bisulfite?
I performed the oxidation with the classical Oxone + NaBr. The original write up calls for a stochio ...
17-9-2014 at 14:05
by: JefferyH
Washing a halogen contaminated aromatic aldehyde with bisulfite?
I have an aromatic aldehyde contaminated with maybe 1-2% its weight in halogen.

Can I add just e ...
17-9-2014 at 11:46
by: JefferyH
Selling my lab
plante1999,

Is there a reason you wanted to sell everything instead of just shipping it over in o ...
14-9-2014 at 06:33
by: JefferyH
Would some alkyl amines have the same properties as ammonia?
I will consider those. I need to consider if a solvent can survive very strong reaction conditions ( ...
14-9-2014 at 05:59
by: JefferyH
Laboratory Rack Mounts? - What is the sales name for this?
[rquote=345289&tid=33532&author=smaerd]PVC is not the most resistant material in the world. ...
13-9-2014 at 19:06
by: JefferyH
Laboratory Rack Mounts? - What is the sales name for this?
Building the frame would probably be the easier part... My delima is finding clamps that are strong ...
13-9-2014 at 16:31
by: JefferyH
Laboratory Rack Mounts? - What is the sales name for this?
They don't look like they would be very "high dollar". In the picture above they look like metal ver ...
13-9-2014 at 16:09
by: JefferyH
Laboratory Rack Mounts? - What is the sales name for this?
None of that is there.....

In case I was being confusing, I am talking mostly about the overall f ...
13-9-2014 at 14:14
by: JefferyH
Laboratory Rack Mounts? - What is the sales name for this?
Those were some of the first terms that I searched for. Can you then link me to a page selling those ...
13-9-2014 at 12:46
by: JefferyH
Laboratory Rack Mounts? - What is the sales name for this?
I've seen these type of things in videos and in for instance the link below:

http://www.ebay.com/ ...
13-9-2014 at 12:00
by: JefferyH
Would some alkyl amines have the same properties as ammonia?
I forgot to mention I still plan to be cooling the reaction mix to well into negative celcius, so th ...
13-9-2014 at 10:56
by: JefferyH
Would some alkyl amines have the same properties as ammonia?
I'm trying to find an alternative to using liquid ammonia for reactions. Liquid ammonia being used t ...
13-9-2014 at 08:44
by: JefferyH
Drying with molecular seives - how fast?
I'm thinking of removing water from solvents like acetone, methanol, ethanol, and so on. Lets say we ...
11-9-2014 at 17:35
by: JefferyH
Drying with molecular seives - how fast?
aga that could also work, depending on how much surface area contact there is. You sound like you ha ...
11-9-2014 at 15:22
by: JefferyH
Drying with molecular seives - how fast?
I've never worked with molecular sieves before but found out how affordable they are and was hoping ...
11-9-2014 at 13:59
by: JefferyH
Performing an Aluminum Amalgam with powdered Aluminum?
Would you say your yields are notably better than reactions performed with foil squares?

As well, ...
10-9-2014 at 18:18
by: JefferyH
Performing an Aluminum Amalgam with powdered Aluminum?
I've never liked amalgams that use foil, messy and the yields are often fairly low. I've read that u ...
10-9-2014 at 15:47
by: JefferyH
Does Hexamine dissolved in water form methyleneimine, or just dissolved Hexamine?
Can Hexamine be dissolved directly in water to give the imine, which can then be further reacted, or ...
4-9-2014 at 20:49
by: JefferyH
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