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toluene --> benzaldehyde
[rquote=678964&tid=2223&author=j_sum1][rquote=678948&tid=2223&author=Waffles SS][b] ...
8-1-2023 at 14:29
by: Johnny Windchimes
carbazole by dehydrogenation of 1,2,3,4-tetrahydrocarbazole on palladium catalyst
Always a treat to read your synth lab notes; a picture's worth 1000 words~!:)

[Edited on 21-12-2022 ...
21-12-2022 at 06:46
by: Johnny Windchimes
I got what you need son....
Truly the best way IMO.

If you cant find HBr, make it from NaBr.

If you cant find 30% H2O2, ma ...
20-12-2022 at 04:42
by: Johnny Windchimes
DIY Vapor Phase Dehydration Machine - Does this Work?
This looks like the ticket for at home chemistry, avoiding chromium compounds and vapour phase setup ...
10-12-2020 at 16:12
by: Johnny Windchimes
Willgerodt-Kindler featuring acetophenone
Nice job! It works with cinnamic acid and styrene if I recall as well, although I've only ever done ...
4-12-2020 at 14:17
by: Johnny Windchimes
DIY Vapor Phase Dehydration Machine - Does this Work?
[rquote=650298&tid=155769&author=Mateo_swe]I read in the disselkamp2008 - Copy.pdf paper "It ...
1-12-2020 at 15:28
by: Johnny Windchimes
Game Chaaaaaanger
If you can prep the Ruthenium on Alumina catalyst which, as of this date of posting, are both fairly ...
1-12-2020 at 12:27
by: Johnny Windchimes
DIY Vapor Phase Dehydration Machine - Does this Work?
That patent's from 1950. Not saying it doesn't work, but give this newer one a look as well. The tem ...
30-11-2020 at 23:52
by: Johnny Windchimes
The unfindable reference for Acetone Dicarboxylic Acid Anhydride
*File was too big to include above*



[file]84874[/file]
30-11-2020 at 14:45
by: Johnny Windchimes
The unfindable reference for Acetone Dicarboxylic Acid Anhydride
[b]@ Boffis:[/b]

If its esters you seek, I'm sure you're aquianted with these fine docs:

It's ...
30-11-2020 at 14:43
by: Johnny Windchimes
The unfindable reference for Acetone Dicarboxylic Acid Anhydride
[rquote=650228&tid=154812&author=kmno4][quote]
R. Kaushall, J. of Indian Chem. Soc., 17, 13 ...
30-11-2020 at 14:09
by: Johnny Windchimes
The unfindable reference for Acetone Dicarboxylic Acid Anhydride
Or.... how About this bad boy?

[i]In eine Losung von 14 g (0,1 Mol) Malonylchlorid[2] in 30 ml Ch ...
30-11-2020 at 13:43
by: Johnny Windchimes
The unfindable reference for Acetone Dicarboxylic Acid Anhydride
[rquote=650220&tid=154812&author=Boffis]Well JW, if it makes you feel any better I have trie ...
30-11-2020 at 13:32
by: Johnny Windchimes
The unfindable reference for Acetone Dicarboxylic Acid Anhydride
[rquote=630498&tid=154812&author=Johnny Windchimes]Hey there,

I'd very much like to stabi ...
30-11-2020 at 11:42
by: Johnny Windchimes
1,3 Acetonedicarboxylic Acid
Unfortunately, I tried these Chinese patent methods (and a few other similar ones with tungstic and ...
30-11-2020 at 11:37
by: Johnny Windchimes
Refining mercury from cinnabar
My turn....

I looked through the whole thread and didn't see this electro process mentioned, so h ...
8-10-2020 at 15:32
by: Johnny Windchimes
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde

[quote]
Again, it's not Gaspa's fault, it's mine, scaling up a procedure from millimoles to mole' ...
2-9-2020 at 19:07
by: Johnny Windchimes
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
[rquote=644066&tid=156115&author=S.C. Wack][rquote=644060&tid=156115&author=Johnny W ...
2-9-2020 at 06:01
by: Johnny Windchimes
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
[rquote=644065&tid=156115&author=clearly_not_atara]Well, the good news is you didn't make ph ...
1-9-2020 at 17:51
by: Johnny Windchimes
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
[rquote=644029&tid=156115&author=clearly_not_atara][rquote=644028&tid=156115&author= ...
1-9-2020 at 15:11
by: Johnny Windchimes
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
[rquote=644029&tid=156115&author=clearly_not_atara][rquote=644028&tid=156115&author= ...
1-9-2020 at 14:20
by: Johnny Windchimes
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
Good day all,

I have not had occasion to do any meaningful chemistry as of late, but I will post ...
31-8-2020 at 18:29
by: Johnny Windchimes
Chemisches Zentralblatt - for free and digitized
156086
26-8-2020 at 16:08
by: Johnny Windchimes
Alternatives to Friedl-Crafts reaction
[rquote=636289&tid=155403&author=goldberg]Thanks. I like idea of using zinc oxide as catalys ...
17-5-2020 at 09:53
by: Johnny Windchimes
Alternatives to Friedl-Crafts reaction
Caveat Emptor on Iranian chemistry IMO, but give this a looksie:

Uses Zinc Oxide instead of AlCl3 ...
17-5-2020 at 07:06
by: Johnny Windchimes
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