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crap yields of phenol-alkyl ether I did another run in 94% EtOH with NaOH to form the phenolate. But we didn't have any more vani ... |
20-8-2005 at 08:14 by: Kalle anka |
crap yields of phenol-alkyl ether Man.. total disaster today when trying to O-alkylate a phenolic compound..
I started out with 10, ... |
9-8-2005 at 13:57 by: Kalle anka |
methyl iodide Nice read Sandmeyer!
I added copper shavings to stabilize the methyl iodide in the storing flask ... |
9-8-2005 at 12:39 by: Kalle anka |
methyl iodide I made methyl iodide myself today.
First i heated 50grams of 85% phosphoric acid at a gas flame. ... |
7-8-2005 at 12:18 by: Kalle anka |
ammonium acetate WOW S.C. Wack!! I saw now that you posted a reply shortly before i completed my last reply. In this ... |
24-6-2005 at 16:13 by: Kalle anka |
ammonium acetate Thanks guys, especially Lambda for your greatly appreciated investment of efforts, this is an unvalu ... |
24-6-2005 at 16:01 by: Kalle anka |
ammonium acetate No, unfortunately I don't have access to any of the articles in the publications of american ch ... |
24-6-2005 at 04:21 by: Kalle anka |
ammonium acetate I tried to pour some of my ammonium acetate solution in acetone, although it is miscible with water ... |
24-6-2005 at 00:30 by: Kalle anka |
Palladium on Charcoal 5%. The catalyst doesn't really help you with releasing hydrogen faster. The reason why it is calle ... |
23-6-2005 at 10:15 by: Kalle anka |
ammonium acetate Thanks esplosivo! I have a heap of CaCl2, but unfortunately it's partially hydrated so i will h ... |
23-6-2005 at 09:33 by: Kalle anka |
ammonium acetate Yesterday i mixed ammonium hydrogen carbonate with an 30% aqueous solution of acetic acid until pH = ... |
23-6-2005 at 03:22 by: Kalle anka |
methyl iodide [quote][i]Originally posted by vulture[/i]
Tertiary alcohols, yes. Secondary, maybe. Primary, no. ... |
16-6-2005 at 00:16 by: Kalle anka |
methyl iodide Cannot the relatively low yields (64%) be due to loss by the volatility of MeI? From my books, makin ... |
14-6-2005 at 15:34 by: Kalle anka |
Acetaldehyde synthesis damn it.. i saw that the Hcl + NaNO3 mixture was a good oxidiser mixture. when NO3 oxidzes something ... |
14-6-2005 at 15:05 by: Kalle anka |
Acetaldehyde synthesis Man! You guys must have written essentially all methods possible to make aliphatic aldehydes. But wh ... |
10-6-2005 at 06:45 by: Kalle anka |