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crap yields of phenol-alkyl ether
I did another run in 94% EtOH with NaOH to form the phenolate. But we didn't have any more vani ...
20-8-2005 at 08:14
by: Kalle anka
crap yields of phenol-alkyl ether
Man.. total disaster today when trying to O-alkylate a phenolic compound..

I started out with 10, ...
9-8-2005 at 13:57
by: Kalle anka
methyl iodide
Nice read Sandmeyer!

I added copper shavings to stabilize the methyl iodide in the storing flask ...
9-8-2005 at 12:39
by: Kalle anka
methyl iodide
I made methyl iodide myself today.

First i heated 50grams of 85% phosphoric acid at a gas flame. ...
7-8-2005 at 12:18
by: Kalle anka
ammonium acetate
WOW S.C. Wack!! I saw now that you posted a reply shortly before i completed my last reply. In this ...
24-6-2005 at 16:13
by: Kalle anka
ammonium acetate
Thanks guys, especially Lambda for your greatly appreciated investment of efforts, this is an unvalu ...
24-6-2005 at 16:01
by: Kalle anka
ammonium acetate
No, unfortunately I don't have access to any of the articles in the publications of american ch ...
24-6-2005 at 04:21
by: Kalle anka
ammonium acetate
I tried to pour some of my ammonium acetate solution in acetone, although it is miscible with water ...
24-6-2005 at 00:30
by: Kalle anka
Palladium on Charcoal 5%.
The catalyst doesn't really help you with releasing hydrogen faster. The reason why it is calle ...
23-6-2005 at 10:15
by: Kalle anka
ammonium acetate
Thanks esplosivo! I have a heap of CaCl2, but unfortunately it's partially hydrated so i will h ...
23-6-2005 at 09:33
by: Kalle anka
ammonium acetate
Yesterday i mixed ammonium hydrogen carbonate with an 30% aqueous solution of acetic acid until pH = ...
23-6-2005 at 03:22
by: Kalle anka
methyl iodide
[quote][i]Originally posted by vulture[/i]

Tertiary alcohols, yes. Secondary, maybe. Primary, no. ...
16-6-2005 at 00:16
by: Kalle anka
methyl iodide
Cannot the relatively low yields (64%) be due to loss by the volatility of MeI? From my books, makin ...
14-6-2005 at 15:34
by: Kalle anka
Acetaldehyde synthesis
damn it.. i saw that the Hcl + NaNO3 mixture was a good oxidiser mixture. when NO3 oxidzes something ...
14-6-2005 at 15:05
by: Kalle anka
Acetaldehyde synthesis
Man! You guys must have written essentially all methods possible to make aliphatic aldehydes. But wh ...
10-6-2005 at 06:45
by: Kalle anka

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