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Here is a guide on how to do it.
Hi Twospoons,
Yes, I have done this successfully before. I wrote a detailed report on how to do ... |
29-3-2024 at 23:49
by: Monoamine |
Separating chloroacetic acid and an sulfuric acid
Thanks for the replies. I will try it with ether then. But distillation also seems like a good optio ... |
18-3-2024 at 15:55
by: Monoamine |
Separating chloroacetic acid and an sulfuric acid
I'm trying out the method from [url=https://patents.google.com/patent/US1304108A/en]this patent[/url ... |
16-3-2024 at 11:52
by: Monoamine |
Solvents for Lithium Hydride
I'm trying to deprotonate the indole nitrogen and subsequently alkylate the nitrogen. I have some Li ... |
29-2-2024 at 21:14
by: Monoamine |
What is needed to store synthesised gasses in gas cylinders
I'm planning to make some MeCl, for a future experiment. The problem is that MeCl is a gas above -24 ... |
25-8-2023 at 21:57
by: Monoamine |
How to make the air in my lab less oxidizing??
I suspect, the bromine in my fridge and the thionyl chloride next to it are partially the culprits. ... |
9-8-2023 at 18:05
by: Monoamine |
How to make the air in my lab less oxidizing??
The air quality in my workspace is pretty terrible, it rusts everything in a matter of days! So it m ... |
4-8-2023 at 08:17
by: Monoamine |
Efficient low tech way to distinguish isomers
what are some ways in which you can distinguish isomers of two molecules that have the same molecula ... |
2-8-2023 at 09:36
by: Monoamine |
Is LiH a strong enough base to deprotonate indole
So I want to protect the indole nitrogen for a reaction, but all I have is LiH and elemental Na (whi ... |
2-8-2023 at 07:58
by: Monoamine |
Preparation of chlorosulfonic acid derived protecting groups
Hi All, I'm currently trying to make some sulfonic acid protecting groups for some upcoming project ... |
1-12-2022 at 11:05
by: Monoamine |
Hydrolysis of alkyl halides
Would NaBH[sub]4[/sub] or LiAlH[sub]4[/sub] reduce aliphatic halogens to H?
For instance would
... |
1-12-2022 at 04:48
by: Monoamine |
Question about amine protection for Grignard reaction
All nice tip! Than you folks. I'll give it a try.  |
4-4-2022 at 08:18
by: Monoamine |
Propionyl chloride with cyanuric chloride and anger
So what's the source of the chlorides? Neither the cyanuric acid, the water, or the propionic acid h ... |
2-4-2022 at 06:42
by: Monoamine |
Stoichiometry for Al(Ga) amalgam reduction of nitroalkane
So I've never done a reduction with an amalgam yet because mercury salts scare the bedoodles out of ... |
1-4-2022 at 20:57
by: Monoamine |
Preparation of Diethyl Sulfate
Impressive work! Thank you for sharing this detailed procedure.
I have a few questions if you do ... |
26-3-2022 at 15:17
by: Monoamine |
Can I open lithium thionyl chloride batteries?
But, yes. Do be careful not to short the battery. You definitely don't want to get splashed with thi ... |
26-3-2022 at 13:54
by: Monoamine |
Can I open lithium thionyl chloride batteries?
It's certainly doable. I did it before and had no issues.
You can read my notes on how to do it h ... |
26-3-2022 at 08:42
by: Monoamine |
Question about Zinc Mercury amalgam safety for Clemmensen reduction
I was wondering if anybody knows how to safely handle and work with Zn(Hg) zinc mercury amalgam for ... |
26-3-2022 at 00:55
by: Monoamine |
Question about amine protection for Grignard reaction
Imagine you need to form a Grignard reagent from a molecule containing both a halogen (from which we ... |
26-3-2022 at 00:27
by: Monoamine |
Question: Storing chlorine in solution
Thank you for all the advice! I also read that sulfuryl chloride can be used as a source of Cl-, as ... |
13-3-2022 at 18:26
by: Monoamine |
Question about SO2 generation
I'm currently trying to make some sulfuryl chloride (SO[sub]2[/sub]Cl[sub]2[/sub]), which can be mad ... |
12-3-2022 at 13:12
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Aaaand... were back.
Ok I did TLC with pure naphthalene and with pure nitrobenzene to see if they ... |
5-3-2022 at 22:47
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
Actually, looking at these again I'm noticing that the brightest (orange) spot is actually still at ... |
5-3-2022 at 17:24
by: Monoamine |
Question about Friedel Crafts acylation and acid chlorides
I used nitrobenzene as the solvent, since it is polar enough to dissolve the AlCl3 complex so the re ... |
5-3-2022 at 17:02
by: Monoamine |
Analysis
So I finally tried this experiment and got a decent looking brown oil that had a smell of orange pee ... |
5-3-2022 at 00:47
by: Monoamine |
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