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Question about amine protection for Grignard reaction
All nice tip! Than you folks. I'll give it a try. :)
4-4-2022 at 08:18
by: Monoamine
Propionyl chloride with cyanuric chloride and anger
So what's the source of the chlorides? Neither the cyanuric acid, the water, or the propionic acid h ...
2-4-2022 at 06:42
by: Monoamine
Stoichiometry for Al(Ga) amalgam reduction of nitroalkane
So I've never done a reduction with an amalgam yet because mercury salts scare the bedoodles out of ...
1-4-2022 at 20:57
by: Monoamine
Preparation of Diethyl Sulfate
Impressive work! Thank you for sharing this detailed procedure.

I have a few questions if you do ...
26-3-2022 at 15:17
by: Monoamine
Can I open lithium thionyl chloride batteries?
But, yes. Do be careful not to short the battery. You definitely don't want to get splashed with thi ...
26-3-2022 at 13:54
by: Monoamine
Can I open lithium thionyl chloride batteries?
It's certainly doable. I did it before and had no issues.

You can read my notes on how to do it h ...
26-3-2022 at 08:42
by: Monoamine
Question about Zinc Mercury amalgam safety for Clemmensen reduction
I was wondering if anybody knows how to safely handle and work with Zn(Hg) zinc mercury amalgam for ...
26-3-2022 at 00:55
by: Monoamine
Question about amine protection for Grignard reaction
Imagine you need to form a Grignard reagent from a molecule containing both a halogen (from which we ...
26-3-2022 at 00:27
by: Monoamine
Question: Storing chlorine in solution
Thank you for all the advice! I also read that sulfuryl chloride can be used as a source of Cl-, as ...
13-3-2022 at 18:26
by: Monoamine
Question about SO2 generation
I'm currently trying to make some sulfuryl chloride (SO[sub]2[/sub]Cl[sub]2[/sub]), which can be mad ...
12-3-2022 at 13:12
by: Monoamine
Question about Friedel Crafts acylation and acid chlorides
Aaaand... were back.

Ok I did TLC with pure naphthalene and with pure nitrobenzene to see if they ...
5-3-2022 at 22:47
by: Monoamine
Question about Friedel Crafts acylation and acid chlorides
Actually, looking at these again I'm noticing that the brightest (orange) spot is actually still at ...
5-3-2022 at 17:24
by: Monoamine
Question about Friedel Crafts acylation and acid chlorides
I used nitrobenzene as the solvent, since it is polar enough to dissolve the AlCl3 complex so the re ...
5-3-2022 at 17:02
by: Monoamine
Analysis
So I finally tried this experiment and got a decent looking brown oil that had a smell of orange pee ...
5-3-2022 at 00:47
by: Monoamine
Triethylsilane
Actually, the method from this paper is for trypropylsilane, but this should be readily adaptable to ...
1-3-2022 at 21:16
by: Monoamine
Yes!
I'm actually super interested in this topic!! I just ordered all the raw materials I need to synthes ...
1-3-2022 at 21:01
by: Monoamine
a novel phenylmorpholine synthesis aka preludin
If preludin is what you want as the end-product, then you may just want to look into obtaining a chl ...
1-3-2022 at 20:49
by: Monoamine
Question: Storing chlorine in solution
I'm wondering if there is a way to make a stable solution of chlorine.

For instance would chlori ...
19-2-2022 at 09:08
by: Monoamine
Question about Friedel Crafts acylation and acid chlorides
Hi Fery, thank you for the link for the reagent supplier! My mouth is watering seeing all the wonder ...
3-2-2022 at 21:42
by: Monoamine
Question about Friedel Crafts acylation and acid chlorides
Thank you for the tips!

I'm planning to use anhydrous AlCl3 as the catalyst. From what I read, th ...
2-2-2022 at 23:05
by: Monoamine
Question about Friedel Crafts acylation and acid chlorides
I'm planning to do my first acylation experiment soon, but I've never done this reaction, so I'm a b ...
2-2-2022 at 05:35
by: Monoamine
Leonid Learner's Book
Hi Basement,

Props for mentioning Leonid Lerners book: "Small scale synthesis of laboratory reag ...
29-1-2022 at 14:01
by: Monoamine
Solvents ?
I really don't understand why people seem to use chlorinated solvents for performing AlCl[sub]3[/sub ...
19-1-2022 at 11:32
by: Monoamine
Question about Grignard reaction
Thank you for all of these valuable tips! Using a Toluene and THF sounds very useful. Also thank you ...
29-12-2021 at 13:31
by: Monoamine
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669165&tid=158187&author=S.C. Wack]Add another SO2.

Also, 2SO3 + SOCl2 -> S2O5 ...
28-12-2021 at 21:43
by: Monoamine
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