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Would it be possible to make 2-bromobenzoyl chloride from salicylic acid
[rquote=564939&tid=114280&author=Loptr][rquote=564925&tid=114280&author=Nakhimov]Dep ... |
19-12-2018 at 10:24
by: Nakhimov |
Would it be possible to make 2-bromobenzoyl chloride from salicylic acid
Depends on what you have available to remove the PG. Probably a benzyl ester.
edit: oops, good po ... |
19-12-2018 at 09:58
by: Nakhimov |
Creating diNitroMethanone from 1,1 diChlorAmino Methanone
If you're fixated on those products, then metal catalysis is the way to go.
Here's a reference yo ... |
19-12-2018 at 09:47
by: Nakhimov |
Creating diNitroMethanone from 1,1 diChlorAmino Methanone
Think of it like nitromethane, but worse. It would proceed through a similar reaction and more readi ... |
19-12-2018 at 09:18
by: Nakhimov |
Would it be possible to make 2-bromobenzoyl chloride from salicylic acid
It would definitely be viable! If I were doing the synthesis in my own lab
1. Protection of carboxy ... |
19-12-2018 at 09:09
by: Nakhimov |
Creating diNitroMethanone from 1,1 diChlorAmino Methanone
If you're synthesizing nitro compounds from carbamide, I would make an effort to detach the amino gr ... |
19-12-2018 at 08:52
by: Nakhimov |
Creating diNitroMethanone from 1,1 diChlorAmino Methanone
If you're looking to synthesize CO2 and NO2 there are much, much safer ways. You're basically using ... |
19-12-2018 at 08:38
by: Nakhimov |
Creating diNitroMethanone from 1,1 diChlorAmino Methanone
I would strongly advise against the synthesis of this particular molecule. I don't think you'd even ... |
19-12-2018 at 08:26
by: Nakhimov |
Chloroform questions
I would expect a mechanism much like this: the reaction would presumably occur twice for each aceton ... |
18-12-2018 at 11:45
by: Nakhimov |
Chloroform questions
Haloform reactions proceed through a keto-enol tautomer, which requires a carbonyl (i.e., not an alc ... |
18-12-2018 at 09:20
by: Nakhimov |
Under what conditions do alkyl azides rearrange to imines?
Here is a recent paper with some in-situ reactions of alkyl azides in the presence of copper catalys ... |
18-12-2018 at 08:33
by: Nakhimov |
Indole
A few possible synthetic routes:
1. o-toluidene and chloroform via formation of an diazonium spec ... |
18-12-2018 at 08:19
by: Nakhimov |
Removing fishy smell from air - possible?
Fish odor is due primarily to methylamine; the acid reacts with the basic amine to form the conjugat ... |
18-12-2018 at 07:54
by: Nakhimov |
Caffeine particles crashed out after saturation - 400mg filled 25ml H2O w/ crystals
Did the solvent cool over time? From the reaction method you described, it's likely you basically ju ... |
18-12-2018 at 07:11
by: Nakhimov |
LiAlH4 vs NaAlH4
The primary reason I've chosen LAH over the sodium species is solubility concerns, NaAlH4 isn't solu ... |
18-12-2018 at 06:33
by: Nakhimov |
Camphor reduction to borneol/isoborneol
[rquote=560161&tid=110282&author=stamasd]
Wondering if it's possible to instead use:
3. Ur ... |
8-12-2018 at 11:19
by: Nakhimov |
