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Determining the Concentration of Dimethylamine in Anhydrous Ethanol
Now I can finally use my buret! It was the first piece of glassware I ever purchased and I am just n ...
19-4-2021 at 13:14
by: Newton2.0
Determining the Concentration of Dimethylamine in Anhydrous Ethanol
Okay, I was assuming you meant acid-base titration but couldn't figure out how it translated to how ...
18-4-2021 at 15:29
by: Newton2.0
Determining the Concentration of Dimethylamine in Anhydrous Ethanol
I know what titration is but don't understand how that tells me what I need to know. Can you explain ...
18-4-2021 at 15:13
by: Newton2.0
Determining the Concentration of Dimethylamine in Anhydrous Ethanol
I had not considered that. So, I could probably try to produce DMA HCl using the 10mL volume I have, ...
18-4-2021 at 13:37
by: Newton2.0
Determining the Concentration of Dimethylamine in Anhydrous Ethanol
I have produced a solution of DMA in EtOH using the DMF/NaOH method. I used 3A mol sieves to remove ...
18-4-2021 at 13:21
by: Newton2.0
Various chlorotoluenes produced during Toluene+TCCA+uv synthesis
As a matter of fact, I do have my eyes set on a few acid chlorides, namely propionyl chloride and bu ...
18-4-2021 at 11:47
by: Newton2.0
Theoretical synthesis of 2-benzyl proline
I was not clear, sorry. Here's what my post meant to say:

Your compound of interest is a ring-con ...
13-4-2021 at 17:22
by: Newton2.0
Nickel Acetate from Nickel Chloride
Yeah, I am going to have to find a way to determine what this is. I'll look and see what tests I can ...
13-4-2021 at 14:20
by: Newton2.0
Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
Your posts are always delightful! Thanks for your hard, diligent work and your thorough posts!
13-4-2021 at 14:08
by: Newton2.0
Theoretical synthesis of 2-benzyl proline
Very interesting! I would expect this thing to have similar pharmacological profile to BZP. It is a ...
13-4-2021 at 13:55
by: Newton2.0
Activating metals post-addition
I do worry that the HCl might attack any deoxybenzoin that forms, either lowering the yield or formi ...
13-4-2021 at 13:50
by: Newton2.0
Activating metals post-addition
I am performing a reduction of benzoin to deoxybenzoin using Zn grains in GAA. The issue I am facing ...
13-4-2021 at 12:40
by: Newton2.0
Nickel Acetate from Nickel Chloride
I was kinda thinking it would be the anhydrous nickel acetate but I could find no reference images. ...
13-4-2021 at 11:00
by: Newton2.0
Nickel Acetate from Nickel Chloride
I have made some Nickel Acetate, however, the finished product is a goldenrod yellow color while the ...
13-4-2021 at 10:45
by: Newton2.0
Metal/acid reduction of benzoin
So, I decided to run the Zn/GAA reduction again but I did not properly activate the Zn grains. As a ...
13-4-2021 at 10:13
by: Newton2.0
What is happening at Deschem?
My recent Deschem purchase has been shipped and it seems to be en route. I hope your order finds you ...
12-4-2021 at 11:31
by: Newton2.0
Various chlorotoluenes produced during Toluene+TCCA+uv synthesis
Excellent! This is a great find! I appreciate this very much. I will make sure to add the appropriat ...
12-4-2021 at 11:28
by: Newton2.0
some questions about triethyl phosphate
This is why we need an international standard for separation of integers and decimals. We write "one ...
1-4-2021 at 04:26
by: Newton2.0
Metasilicates
Cool! is there a difference in color if you create the anhydrous metal metasilicates (or orthosilica ...
25-3-2021 at 10:44
by: Newton2.0
Using enormous excess of solvents for extractions?
I had a huge problem with that at first! It wasn't mechanically intuitive how much of any reagent a ...
25-3-2021 at 10:34
by: Newton2.0
Various chlorotoluenes produced during Toluene+TCCA+uv synthesis
I recognize now that the way I would get ring-substituted chlorine is with the addition of FeCl3 and ...
25-3-2021 at 10:27
by: Newton2.0
(safer) fluorination of benzaldehyde?
You've probably figured this out, but depending on your location, there are places that offer 3-F-be ...
23-3-2021 at 18:53
by: Newton2.0
Making a lab stand/rack setup - what is a good design?
I'm an electrician, so I basically took strut and made a square frame from which I hung some all-thr ...
23-3-2021 at 16:24
by: Newton2.0
lefetamine
I see about 12 immediate analogues for the rest of the benzoin I have.
13-3-2021 at 13:49
by: Newton2.0
lefetamine
Whoops, that's my bad guys on both counts, namely, beating the dead horse of lefetamine on this foru ...
13-3-2021 at 12:35
by: Newton2.0
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