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reduction of carboxylic acid without hydride
Conversion to an amide, dehydration to a nitrile, and reduction with SnCl2/HCl to an aldehyde?

ED ...
23-12-2016 at 17:16
by: NitreRat
Trying to synthesize 1-iodobutane
There are loads of different easy-to-aquire oxidizing agents that can oxidize KI into elemental iodi ...
4-11-2016 at 08:18
by: NitreRat
Benzaldehyde on Amazon Prime?
[rquote=465872&tid=70340&author=Maroboduus]I always confuse those two. Ethyl nitrate's the ...
2-11-2016 at 20:17
by: NitreRat
Oxidation of styrene to phenylacetaldehyde
[rquote=465850&tid=22421&author=gravityzero]After reading the thread in full, it is still un ...
2-11-2016 at 18:35
by: NitreRat
Raspberry Ketone Synthesis
The ketone could be converted to an acetal then you could hydrogenate the double bond under basic co ...
20-6-2016 at 04:57
by: NitreRat
Halobenzenes by decarboxylation of halobenzoic acids
@notoxicshit
Do you have a reference for the halogenation of benzoic acids with hypochlorites?
Mos ...
11-6-2016 at 13:14
by: NitreRat
Anyone else interestead in extracting chemicals from plant material?
Sorry, my mistake. I didn't see ficolas' posts so I thought it was a whole thread of you talking to ...
9-6-2016 at 06:54
by: NitreRat
Anyone else interestead in extracting chemicals from plant material?
...ummm... am I missing something here?
9-6-2016 at 06:39
by: NitreRat
Production of chiral alcohol enantiomers
[rquote=451199&tid=66452&author=CharlieA]do you have a reference to the MEK reduction with y ...
9-6-2016 at 03:27
by: NitreRat
Broken Vigreux Column
It could be used in a simple distiallation set-up as a final precausionary condenser after the recei ...
4-6-2016 at 15:18
by: NitreRat
Pyrrolidine/Putrescine?
[rquote=450779&tid=66419&author=morsagh]So in synthesis of secondary amines can be used N su ...
4-6-2016 at 14:51
by: NitreRat
Pyrrolidine/Putrescine?
If your desired product is 1,4-diaminobutane you could use potassium phthalimide in the Gabriel synt ...
4-6-2016 at 10:21
by: NitreRat
Could Phenyl triflate undergo nucleophilic substitution?
While most aliphatic alcohols can easily be converted to the corosponding alkyl halide with a the ap ...
3-6-2016 at 19:55
by: NitreRat
Yellow ether ?
Sounds like a trace aldol condensation contaminant. What was your source of ethanol? I don't know if ...
3-6-2016 at 10:31
by: NitreRat
New chemicals for sale !
Recently received my order from mario48. A pleasure to deal with and I can highly recommend them to ...
27-5-2016 at 11:16
by: NitreRat
Vacuum Desiccator vs Rotary Evaporator
Rotovaps are capable of removing much more solvent than most vacuum desiccators are capable of. Vacu ...
24-5-2016 at 09:02
by: NitreRat
Amphetamine from Cinnamaldehyde
According to this paper I found in the Rhodium archives [url=https://www.erowid.org/archive/rhodium/ ...
10-5-2016 at 10:19
by: NitreRat
Amphetamine from Cinnamaldehyde
You're right Chemi Pharma, my apologies.

But perhaps I can offer a little help. I imagine the dif ...
10-5-2016 at 09:26
by: NitreRat
Fun/cool reactions/experiments to do with CS2?
You could make some Carbon tetrachloride and use it to write your name into the ozone layer
9-5-2016 at 18:50
by: NitreRat
Labware and chemical recommendations
[rquote=448381&tid=65971&author=j_sum1]Insulated column has a gentler thermal gradient over ...
9-5-2016 at 17:05
by: NitreRat
Labware and chemical recommendations
[rquote=446122&tid=65971&author=MrMario]Same setup as simple distillation but with an additi ...
9-5-2016 at 14:51
by: NitreRat
Amphetamine from Cinnamaldehyde
Whilst I don't think this thread deserves as much attention as it has, I stumbled upon this paper ea ...
9-5-2016 at 11:06
by: NitreRat
New OTC UK source of Chlorobenzene
It seems strange to me that they won't ship toluene or dichloroethane without all the right paperwor ...
9-5-2016 at 10:41
by: NitreRat
New OTC UK source of Chlorobenzene
Recently APC Pure has added some useful chemicals to their Catalogue such as Acetophenone, Acetonitr ...
9-5-2016 at 07:51
by: NitreRat
Defluorodation(?) of substituted fuorobenzenes to benzenes.
[rquote=448217&tid=66181&author=CuReUS]Raney Ni in the presence of NaOH can remove F from be ...
8-5-2016 at 04:49
by: NitreRat
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