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Blanc chloromethylation employing iodine
[rquote=644264&tid=156134&author=ArbuzToWoda]
A bit of an offtopic here, but obtaining 1,4- ...
6-9-2020 at 21:54
by: RadicallyStabilized
Caution: Making bromine from TCCA and ammonium bromide does not work
Just a short addendum how I disposed of the unreacted TCCA. It is an oxidant, harmful for aquatic or ...
4-9-2020 at 05:18
by: RadicallyStabilized
Caution: Making bromine from TCCA and ammonium bromide does not work
[rquote=643911&tid=156107&author=beta4]
So you may have inadvertently made a small amount o ...
30-8-2020 at 05:44
by: RadicallyStabilized
Caution: Making bromine from TCCA and ammonium bromide does not work
I attempted to make some bromine using NileRed's method with TCCA and HCl (https://www.youtube.com/w ...
30-8-2020 at 04:14
by: RadicallyStabilized
Chloroacetic acid from glycine or another bullshit patent?
Very well done. How about a little more detailed writeup including quantities and yield? I'd like to ...
14-8-2020 at 06:49
by: RadicallyStabilized
Chloroacetic acid from glycine or another bullshit patent?
I have done this reaction and it runs well. The problem, as stated in the patent, is the isolation o ...
3-8-2020 at 22:24
by: RadicallyStabilized
Nitrates in decent yield from the oxidation of melamine by calcium hypochlorite
[rquote=641107&tid=155631&author=symboom]Nope even that's getting rare you just have to stoc ...
20-7-2020 at 23:08
by: RadicallyStabilized
Nitrates in decent yield from the oxidation of melamine by calcium hypochlorite
[rquote=639763&tid=155631&author=Bromolone]Alternative sources to nitrates are the need of t ...
19-7-2020 at 22:34
by: RadicallyStabilized
Benzoin condensation using hydrogen cyanide?
[rquote=637889&tid=155502&author=DavidJR]
I tried the thiamine method, and it did work, but ...
8-6-2020 at 07:24
by: RadicallyStabilized
Cosmetics Chemistry
Hand creams are considered the holy grail of home cosmetics for a reason. I have made some a few tim ...
29-5-2020 at 23:08
by: RadicallyStabilized
Mercury sources in EU?
[rquote=635271&tid=155306&author=morganbw]
If my memory has not failed me I think I thought ...
4-5-2020 at 03:37
by: RadicallyStabilized
benzyl alcohol oxidation
No, I haven't forgotten, but the amount of water in my first try was much less than what was used in ...
19-3-2020 at 00:09
by: RadicallyStabilized
benzyl alcohol oxidation
OK, thank you, clearly_not_atara.

Please see my post from 2020-3-10 where I used DCM and very lit ...
18-3-2020 at 09:31
by: RadicallyStabilized
benzyl alcohol oxidation
@Chemi Pharma: Thanks. Unfortunately I don't have any Al2O3 right now. Still I don't get how TBAB is ...
18-3-2020 at 07:38
by: RadicallyStabilized
benzyl alcohol oxidation
Thanks for the clarification! I agree with your ideas about the workup. I only dried the organic pha ...
11-3-2020 at 03:29
by: RadicallyStabilized
benzyl alcohol oxidation
OK, I tried this and got a spectacularly shitty yield.

Lab notes start:

32.8 g (0.15 mol) of s ...
10-3-2020 at 10:58
by: RadicallyStabilized
benzyl alcohol oxidation
Chemi Pharma, thanks for the reply. Sounds reassuring.

I will give this a try and report back (th ...
8-3-2020 at 05:54
by: RadicallyStabilized
benzyl alcohol oxidation
I wonder whether the method outlined by Chemi Pharma is really going to work.

First, if using TBA ...
7-3-2020 at 01:20
by: RadicallyStabilized
Fuchsin confusion
Cool that you took the time to investigate this! I wonder where the bubbles/foam comes from though. ...
28-2-2020 at 00:06
by: RadicallyStabilized
Fuchsin confusion
Now this thread has evolved from "fuchsin confusion" to "bisulfite confusion"...

I'm not really s ...
19-2-2020 at 01:33
by: RadicallyStabilized
Fuchsin confusion
It's in the German wikipedia: https://de.wikipedia.org/wiki/Natriumhydrogensulfit

If my German do ...
18-2-2020 at 06:29
by: RadicallyStabilized
Fuchsin confusion
Ok, seems to work, good.

Are you sure you've got the bisulfite NaHSO3? Wikipedia says it's only s ...
18-2-2020 at 02:01
by: RadicallyStabilized
Fuchsin confusion
You probably need to add more (meta)bisulfite.

I just tested my basic fuchsine (which I bought ye ...
17-2-2020 at 04:39
by: RadicallyStabilized
Chlorate or perchlorate?
Thanks for the quick reply.

The methylene blue test gave no color change.

The sugar/H2SO4 test ...
16-2-2020 at 09:42
by: RadicallyStabilized
Chlorate or perchlorate?
Hi,
I guess one of the more energetic users here might know this...

I have inherited an old reag ...
16-2-2020 at 06:36
by: RadicallyStabilized
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