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purification of LAH
I know this sounds lame, but buy more if its been sitting around for a while....
story of mine is ... |
16-4-2011 at 16:44
by: RiP057 |
McLeod Gauge
what do you think about the price??? did I get a steal or what???? |
16-4-2011 at 09:42
by: RiP057 |
McLeod Gauge
finally someone with some solid advice, I think I will start off with the 30% which is still pretty ... |
16-4-2011 at 08:57
by: RiP057 |
Has anyone made sodamide?
why not use benzene as a solvent??? I know it wouldnt solvate it very much, but it would a little |
15-4-2011 at 21:58
by: RiP057 |
Has anyone made sodamide?
very true if you cool the cylinder down and then invert it and open up it usually comes out liquid o ... |
15-4-2011 at 21:53
by: RiP057 |
McLeod Gauge
thats actually a lot of work, I like what I was taught which was conc HNO3, but for safety's sake ca ... |
15-4-2011 at 17:37
by: RiP057 |
McLeod Gauge
uhhh duhh!!!
but in better scientific prose....
only an amateur would dare mess with the highl ... |
15-4-2011 at 15:25
by: RiP057 |
McLeod Gauge
Im going to give it a try first with the dilute then ramp it up if nothing occurs. As far as the ga ... |
15-4-2011 at 07:00
by: RiP057 |
McLeod Gauge
so your recommending dilute nitric, and there is a little Hg left in the left most capillary where t ... |
14-4-2011 at 20:59
by: RiP057 |
McLeod Gauge
I have recently aquired a swiveling McLeod Gauge
much like this one
[img]https://fscimage.fishersc ... |
14-4-2011 at 19:55
by: RiP057 |
malachite green
[rquote=191595&tid=14768&author=entropy51]
I knew a chemist who once said that anyone who t ... |
30-10-2010 at 17:46
by: RiP057 |
HI reductions, no red P
Nicoderm has gotten on me for references, but that usually requires access
Huaxue Fanying Gongche ... |
29-10-2010 at 15:51
by: RiP057 |
Benzene --> benzaldehyde
it would seem I am talking out of my arse, but in this journal article it was accomplished
Tetrahed ... |
29-10-2010 at 15:37
by: RiP057 |
Benzene --> benzaldehyde
will do going to do a search on beilstein after I shower.... I figure most people have access to so ... |
29-10-2010 at 12:49
by: RiP057 |
Feasible Reactions?
I am a distillation freak, and I must admit I want crystal clear indoles when I am working on them, ... |
28-10-2010 at 17:12
by: RiP057 |
HI reductions, no red P
From what I see benzoquinone through tautemerization would protonate at the O leaving a positive car ... |
28-10-2010 at 17:04
by: RiP057 |
Benzene --> benzaldehyde
benzene will readily undergo the vilsmeier hack just like it will undergo chlorination iodination ni ... |
28-10-2010 at 16:35
by: RiP057 |
Benzene --> benzaldehyde
I thought vilsmeier hack was the way to go to make benzaldehydes???
simple DMF/POCl3 reaction wit ... |
27-10-2010 at 20:03
by: RiP057 |
Book for application of computer in chemistry
cramers book is the best he is a phenomenal computational chemist.... |
27-10-2010 at 10:46
by: RiP057 |
Feasible Reactions?
synthesis of 2-methylindole is not the hard part I have no distillation setup at the moment so that ... |
27-10-2010 at 10:26
by: RiP057 |
Free online Gaussian
fail you could get the entire university banned from gaussian
check out
bannedbygaussian.org |
26-10-2010 at 20:28
by: RiP057 |
Rotational barrier calculations
why use jaguar and not use gaussian???
if you were using gaussian I could help you all day... its ... |
26-10-2010 at 20:23
by: RiP057 |
Feasible Reactions?
I agree zed the best way to do things is DIY... any number of reagents is outrageous in price or in ... |
26-10-2010 at 19:02
by: RiP057 |
Catechol preparation
[rquote=190128&tid=293&author=peach] just buy a bottle of the crap.
[Edited on 13-10-2010 b ... |
26-10-2010 at 18:28
by: RiP057 |
Synthesis of p-aminobenzoic acid from benzyl alcohol
[rquote=191273&tid=14713&author=not_important]
same as toluene, so the iodination will need ... |
26-10-2010 at 18:13
by: RiP057 |
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