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Separation of Nitroethane from Methoxy-2-propanol
[rquote=516139&tid=82269&author=Tsjerk][rquote=516052&tid=82269&author=SamuelLFracti ...
30-4-2018 at 14:04
by: SamuelLFraction
Separation of Nitroethane from Methoxy-2-propanol
Tsjerk I don’t know how I haven’t come across that proxy before but thank you very much for that ...
29-4-2018 at 14:44
by: SamuelLFraction
Separation of Nitroethane from Methoxy-2-propanol
Unforunately oxidation to Methoxy 2 Propanone is not beneficial as the BP actually drops to 118 :(
29-4-2018 at 10:46
by: SamuelLFraction
Separation of Nitroethane from Methoxy-2-propanol
Amoled, thanks for the information, I hate how they subject you to ridiculous payments. Perhaps some ...
29-4-2018 at 08:11
by: SamuelLFraction
Separation of Nitroethane from Methoxy-2-propanol
At this point in time Melgar the challenge is in the ability to selectively separate these two compo ...
29-4-2018 at 00:48
by: SamuelLFraction
Separation of Nitroethane from Methoxy-2-propanol
The problem being if a ternary azeotrope is formed between water, M2P and Nitroethane. Of course tha ...
28-4-2018 at 13:47
by: SamuelLFraction
Separation of Nitroethane from Methoxy-2-propanol
Thank you Tsjerk for the info on M2P. Now that it’s confirmed to have an azeotrope with water, it ...
28-4-2018 at 12:21
by: SamuelLFraction
Separation of Nitroethane from Methoxy-2-propanol
Finally I have managed to find an OTC source of EtNO2, no more endless and expensive work ups! Well. ...
27-4-2018 at 15:43
by: SamuelLFraction
Ethyl Iodide
Thank you Melgar, Silicon would most certainly be an interesting reagent to use. I'll be adding elem ...
28-11-2017 at 13:12
by: SamuelLFraction
Ethyl Iodide
Finishing the procedure calling for 84% alcohol has resulted in a cloudy distillate with a boiling p ...
28-11-2017 at 03:37
by: SamuelLFraction
Ethyl Iodide
@ S.C Wack, oh well, I suppose in chemistry not everything works out to how you expect. Yes I have r ...
25-11-2017 at 09:49
by: SamuelLFraction
Ethyl Iodide
@S.C Wack, this may well explain why low yield then, since anhydrous ethanol was used. I will try th ...
25-11-2017 at 08:36
by: SamuelLFraction
Ethyl Iodide
@Chemi Pharma, I did originally think it would be a lot easier to avoid the Aluminium route and go w ...
25-11-2017 at 02:37
by: SamuelLFraction
Ethyl Iodide
Zts - thank you for your reply, I feel a bit silly now realising this haha!
AvB - I'm glad to have ...
24-11-2017 at 14:57
by: SamuelLFraction
Ethyl Iodide
Hi guys, after some lurking I've decided to finally post something ;)

Having a bit of an issue un ...
24-11-2017 at 13:52
by: SamuelLFraction

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