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Syringol from pyrogallol
[rquote=641047&tid=155756&author=goldberg]@TheMasterOfTheInternet: Finally i would like atta ... |
18-7-2020 at 13:14
by: TheMasterOfTheInternet |
Swarm ideas needed: Many chemicals but little time: What's the most amazing stuff to make within one day?
[rquote=641005&tid=155829&author=njl]You could try a mitromethane based explosive. Tech ingr ... |
17-7-2020 at 17:39
by: TheMasterOfTheInternet |
Syringol from pyrogallol
[rquote=640216&tid=155756&author=karlos³]Syringol is a phenol so it should be easy to separ ... |
17-7-2020 at 17:25
by: TheMasterOfTheInternet |
NaCl vs. KCl to salt out oganics
[rquote=641003&tid=155826&author=FormerBeagle]TMOTI: yes, thanks that is a very useful sugge ... |
17-7-2020 at 17:02
by: TheMasterOfTheInternet |
Almost getting caught
[rquote=638555&tid=155603&author=NonEthicalPyrotechnics]I'm sorta new to energetic chemistry ... |
17-7-2020 at 16:38
by: TheMasterOfTheInternet |
Swarm ideas needed: Many chemicals but little time: What's the most amazing stuff to make within one day?
Hi thfere!
[b]I have access to a wet dream of[/b]
~15kg KNO3
65% Oleum
98% Sulfuric acid
30% ... |
17-7-2020 at 15:52
by: TheMasterOfTheInternet |
NaCl vs. KCl to salt out oganics
NaCl and KCl are almost identical when salting out organics from water.
KCl should be slightly bett ... |
17-7-2020 at 15:11
by: TheMasterOfTheInternet |
NaCl vs. KCl to salt out oganics
-deleted-
[Edited on 18-7-2020 by TheMasterOfTheInternet] |
17-7-2020 at 14:56
by: TheMasterOfTheInternet |
Tryptamine and formaline at room temperature
Update:
The product does NOT dissolve in 25% acetic acid, even when boiling for >30min.
The oil ... |
18-3-2019 at 15:28
by: TheMasterOfTheInternet |
Failed nitro-aldol reaction. Possible cause and fix?
I can easily tell you the difference between MeOH, EtOH and IPA, I've used them all for NaBH4 reduct ... |
18-3-2019 at 15:23
by: TheMasterOfTheInternet |
Failed nitro-aldol reaction. Possible cause and fix?
NiCl2+NaBH4 and Ra-Ni+NaBH4 both have a slightly tricky workup and if the reaction time was too shor ... |
17-3-2019 at 15:01
by: TheMasterOfTheInternet |
Tryptamine and formaline at room temperature
Tryptamine is a quite strong base on its own, so a trazine I a very good guess I think
I the mean ... |
16-3-2019 at 19:18
by: TheMasterOfTheInternet |
Storing over drying agents - degradation?
[quote]
Since it seems molecular sieves are much more commonly used for storage, do they have a she ... |
16-3-2019 at 19:02
by: TheMasterOfTheInternet |
Storing over drying agents - degradation?
Once I was storing elderly THF over sodium shavings. After some months some clear yellowish gel was ... |
16-3-2019 at 18:55
by: TheMasterOfTheInternet |
Al/NiCl2*6H2O: OTC hydride-like reactivity
[rquote=605452&tid=65915&author=Loptr]The title of the paper claims it is a neutral reducing ... |
16-3-2019 at 18:50
by: TheMasterOfTheInternet |
Is it possible to synthesise Pd/C from home?
I've made Pd/C, Pt/C, Ra-Ni and Nickel boride catalysts several times on my own.
And to answer your ... |
14-3-2019 at 17:35
by: TheMasterOfTheInternet |
Tryptamine and formaline at room temperature
The caramal sauce solidifed in the fridge in the meanwhile
[quote]
...i had read about some primar ... |
14-3-2019 at 08:46
by: TheMasterOfTheInternet |
carboxylation of skatole
Here's the German original (directly from the stone-age  )
http://sci-hub.se/https://onlinelibrary ... |
13-3-2019 at 23:02
by: TheMasterOfTheInternet |
carboxylation of skatole
Potassium permanganate, sodium dichromate and several other oxidants will oxidise the -CH3 to -COOH ... |
13-3-2019 at 22:41
by: TheMasterOfTheInternet |
Tryptamine and formaline at room temperature
[rquote=605253&tid=146432&author=Assured Fish]At best you would have formed an imine, at wor ... |
13-3-2019 at 21:46
by: TheMasterOfTheInternet |
Tryptamine and formaline at room temperature
Hi!
I've just dissolved 1g tryptamine (98% synthesis grade) in about 5-6mL MeOH (99%) and added a l ... |
13-3-2019 at 03:12
by: TheMasterOfTheInternet |
