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Diethylamine Synthesis
For the small chance that anyone was interested in my experimentation with the ethanolic DEET and aq ...
6-9-2012 at 01:41
by: The_Natural
Diethylamine Synthesis
ok so the ethanol should have been removed prior.. glad i didnt decide to boil away whats left of th ...
6-3-2010 at 17:03
by: The_Natural
Diethylamine Synthesis
To approximately 50 grams of deet in 50-60 grams of ethanol was added 50 grams of conc. H2SO4 in 100 ...
5-3-2010 at 16:10
by: The_Natural
Magnetic stirring in a 5L Flask
Magnet stirring is indeed adequate, but vigorous it isn't. Mechanical stirring will be the future.
...
17-3-2009 at 04:03
by: The_Natural
Magnetic stirring in a 5L Flask
Before I make the acquisition.

Will I be able to magnetically stir non-viscous reactions fluids o ...
14-11-2008 at 17:22
by: The_Natural
DCM or Et2O?
If AcOEt is substituted for DCM/Chloroform in a biphasic NaOCl oxidation system would significant am ...
10-9-2008 at 15:31
by: The_Natural
thf oxidation
Oxidation systems utilizing H2O2 catalyzed by a group 6 metal ion and a PTC oxidize secondary alcoho ...
13-7-2008 at 18:50
by: The_Natural
thf oxidation
I'm sure no one is interested in where I'm from or what I do.

There is a follow up article to the ...
21-6-2008 at 05:56
by: The_Natural
thf oxidation
Sweet, maybe after a few days I might have 1 ml.

This would not be enough to clean the ports on m ...
19-6-2008 at 15:29
by: The_Natural
thf oxidation
Yes.. I have read the paper, thanks for asking ;)

Yes.. the patent contains some useful details o ...
19-6-2008 at 04:25
by: The_Natural
thf oxidation
Solvent free permanganate oxidation of THF to GBL (Tet letters 42, 2001)

http://www.erowid.org/ar ...
18-6-2008 at 17:30
by: The_Natural
vacuum system controlled leak or control
Please excuse my lack of knowledge on the subject.

I read the other thread in which you described ...
28-5-2008 at 21:34
by: The_Natural
vacuum system controlled leak or control
Interesting, I already have the mercury and some spare 1 ml pipettes.

Can pipettes be bent when h ...
25-5-2008 at 22:30
by: The_Natural
vacuum system controlled leak or control
Do you think this could actually work? Using a compound of known boiling point to calibrate the vacu ...
25-5-2008 at 03:28
by: The_Natural
vacuum system controlled leak or control
I have a 3 cfm, 75 micron vacuum pump to be used in a dst. setup using flat bottom, round reaction f ...
22-5-2008 at 18:25
by: The_Natural

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