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N-isopropyl-2-propanimine preparation
Then he should use IPA.
The purpose of refluxing is to form the imine. It's a simple enough opera ... |
22-12-2015 at 03:34
by: User123 |
N-isopropyl-2-propanimine preparation
Hence I advised him to reflux the toluene to form the imine, then distill the toluene to dry the IMI ... |
22-12-2015 at 03:25
by: User123 |
N-isopropyl-2-propanimine preparation
I don't know anything about mechanistic studies of uncatalysed imine formation. Here's an example of ... |
22-12-2015 at 02:45
by: User123 |
N-isopropyl-2-propanimine preparation
The reasons are clearly not obvious to me, so perhaps you could make them so?
As for it not being ... |
22-12-2015 at 01:36
by: User123 |
Condenser pump
A nice makeshift way of having a running water source is to use two aspirator bottles:
https://stat ... |
21-12-2015 at 23:15
by: User123 |
Mantle with no heat?
You can get solid blocks of iron which are flask-shaped and designed to go on top of a hotplate/stir ... |
21-12-2015 at 16:54
by: User123 |
youtube
Those are some useful videos. Thanks for the recommendations, and to the people who made them. I've ... |
21-12-2015 at 12:27
by: User123 |
N-isopropyl-2-propanimine preparation
Thinking about it, you may need to reflux it for a little bit before distilling it off, to give the ... |
21-12-2015 at 12:17
by: User123 |
N-isopropyl-2-propanimine preparation
No, it doesn't. The removal of water as an azeotrope will drive the reaction forward on its own.
I ... |
21-12-2015 at 11:15
by: User123 |
The Short Questions Thread (4)
You'd just have a flask with acetone hydrazone dissolved in ethylene glycol. To that you would add N ... |
21-12-2015 at 11:07
by: User123 |
The Short Questions Thread (4)
The scheme is incomplete. It uses a strong base such as sodium hydroxide to abstract the hydrogens o ... |
21-12-2015 at 10:36
by: User123 |
Stuff to Pick Up at Chem Supplier
Do you use P2O5 as a reagent, or just as a dessicant? As far as I know, using separate beakers of Na ... |
21-12-2015 at 08:42
by: User123 |
Stuff to Pick Up at Chem Supplier
I am a bit confused as to why you need to ask. If you are competent enough to be using lithium alumi ... |
21-12-2015 at 04:23
by: User123 |
N-isopropyl-2-propanimine preparation
Imines can form in DCM, but it will not be quantitative. If you want to be sure of imine formation y ... |
21-12-2015 at 02:03
by: User123 |
New Sheriff in Town
What is the point in you, aga? |
19-12-2015 at 19:38
by: User123 |
New Sheriff in Town
Bert: bfesser took it upon himself to delete vast swathes of posts going back years; to edit other p ... |
19-12-2015 at 13:54
by: User123 |
New chemicals for sale !
I've made several orders with Mario now, and I'd just like to say that I have been impressed every t ... |
19-12-2015 at 08:17
by: User123 |
New Sheriff in Town
I find some of his views a bit out there, but there is no physical limit to how many threads there c ... |
19-12-2015 at 07:54
by: User123 |
New Sheriff in Town
[rquote=431814&tid=64699&author=woelen][rquote=431742&tid=64699&author=User123]Bfess ... |
19-12-2015 at 07:42
by: User123 |
New Sheriff in Town
He gave an example of what he views as a 'pile of nonsense'. No straw man involved. |
17-12-2015 at 19:31
by: User123 |
New Sheriff in Town
So you intend to actively piss off franklyn, whose posts and sceptical attitude many of us like? |
17-12-2015 at 19:25
by: User123 |
New Sheriff in Town
[rquote=431744&tid=64699&author=Amos][rquote=431742&tid=64699&author=User123]Bfesser ... |
17-12-2015 at 18:55
by: User123 |
New Sheriff in Town
Bfesser pissed off just about every older member of this forum with his excessive pestering and gett ... |
17-12-2015 at 18:51
by: User123 |
Organic Goal
Rather than just making 'something', why not prepare some useful reagents, or solvents? I don't know ... |
17-12-2015 at 15:32
by: User123 |
Bornyl chloride as alkylating agent?
You ARE wrong... Because you didn't read Nicodem's post. Neither did blogfast25. He has answered all ... |
17-12-2015 at 05:36
by: User123 |
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