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Nitration and acetone
I would think that nitric acid would initially go after the alpha carbons and oxidize the ketone to ...
30-1-2021 at 21:11
by: Yamato71
ETN synthesis without H2SO4
33 ml of WFNA will esterify 10 g of pentaerythritol with excellent yields without the need for SA. ...
30-1-2021 at 20:45
by: Yamato71
Selenium Nitride
You can easily dry benzene by azeotropic distillation. Benzene forms a low boiling (69.5C) azeotrop ...
30-1-2021 at 18:25
by: Yamato71
Potential lowcost/portable/civilians available 2 shot electric blasting machine
Commercial blasting machines of the 10 cap variety usually generate 90-150 volts DC at a relatively ...
30-1-2021 at 18:13
by: Yamato71
Life after detonation
I know, I said that I'm signing off, but there's a bit of unfinished business to take care of....

...
15-1-2021 at 20:29
by: Yamato71
Life after detonation
Hello everyone! I hope all of you have managed to stay relatively safe and healthy during this dump ...
5-12-2020 at 21:30
by: Yamato71
Life after detonation
It has been a long painful road, but as conventional wisdom reminds us, "What doesn't kill you makes ...
12-2-2020 at 15:53
by: Yamato71
Life after detonation
Thanks Xeon, it's damn good to be back.
12-2-2020 at 13:42
by: Yamato71
Life after detonation
Hello group, I recently observed (somehow the word "celebrated" doesn't seem appropriate) the ninth ...
11-2-2020 at 18:30
by: Yamato71
DIAMINOURONIUM (DI)NITRATE
I've described my experience with fumed silica in another thread since it doesn't relate directly to ...
20-6-2019 at 16:33
by: Yamato71
Non Newtonian mixtures using fumed silica
This thread was split from the DIAMINOURONIUM (DI)NITRATE thread.

The project that resulted in my ...
20-6-2019 at 16:12
by: Yamato71
DIAMINOURONIUM (DI)NITRATE
If this product feels more comfortable existing as an oil after nitration, who are we to insist that ...
15-6-2019 at 23:21
by: Yamato71
What do you think I should do with my picric acid?
I have always been of the opinion that the words "pressing" and "primaries" should never be uttered ...
12-2-2019 at 07:34
by: Yamato71
Life after detonation
Yes, it was 50 grams dissolved in 500 ml of hot MeOH.
12-2-2019 at 05:57
by: Yamato71
Life after detonation
Jeez the years keep ticking off faster and faster. I'm officially OLD. I turned 65 last November a ...
11-2-2019 at 21:59
by: Yamato71
Soxhlet
You have to remember that the extraction chamber has more than solvent in it. There is also the thi ...
18-8-2018 at 08:10
by: Yamato71
FS Schlenk manifold, 24/40 glassware, 45/50 cold trap
No problem with the missing nut on the Schlenk manifold. The manufacturer obviously anticipated thi ...
18-8-2018 at 07:47
by: Yamato71
Life after detonation
Well, another year gone and I'm hanging in there. I'll update when I get a little more time.
5-11-2017 at 10:57
by: Yamato71
Uranium Extraction from Vaseline Glass Help
My experience with uranium glass goes back a while. In the 30's and 40's, neon sign makers used a g ...
13-2-2017 at 20:58
by: Yamato71
Uranium Extraction from Vaseline Glass Help
My experience with uranium glass goes back a while. In the 30's and 40's, neon sign makers used a g ...
13-2-2017 at 20:56
by: Yamato71
UO2 looking for ways to react it
When prospecting for uranium containing rare earth minerals at night in Texas, I carry an ultraviole ...
4-2-2017 at 19:41
by: Yamato71
Uranium Extraction from Vaseline Glass Help
There is a very good reason that high level nuclear waste is vitrified into glass before disposal. ...
4-2-2017 at 19:31
by: Yamato71
zinc peroxide
Back in the day, lab methods for the production of concentrated H2O2 as well as metallic and organic ...
1-2-2017 at 06:15
by: Yamato71
What the hell did I just make?
@ j_sum1 I just finished reading your posts detailing your efforts to synthesize anhydrous NO2 with ...
28-11-2016 at 07:09
by: Yamato71
What the hell did I just make?
In looking at the ring structure of DCCA salts it seems likely that another hideously toxic compound ...
28-11-2016 at 04:29
by: Yamato71
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