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Silver and Copper Cyanide from Potassium Ferrocyanide
[rquote=293656&tid=24764&author=kmno4]I have made few experiments on 7,5g CuSO4•5H2 ... |
1-8-2013 at 11:46
by: anomolous |
Silver and Copper Cyanide from Potassium Ferrocyanide
Well, I tried it out and its not quite as simple as I thought it would be. Here are the results.
... |
12-7-2013 at 11:17
by: anomolous |
Silver and Copper Cyanide from Potassium Ferrocyanide
[rquote=289430&tid=24764&author=Random]Anomolous, isn't that too much cyanogen right there? ... |
25-6-2013 at 13:45
by: anomolous |
Silver and Copper Cyanide from Potassium Ferrocyanide
Here is a similar reaction for making Copper (I) Chloride from "Handbook of Preparative Inorganic Ch ... |
24-6-2013 at 16:30
by: anomolous |
Silver and Copper Cyanide from Potassium Ferrocyanide
Here is a basic outline of how I plan on doing this reaction. Please feel free to chime in with reco ... |
24-6-2013 at 06:19
by: anomolous |
Silver and Copper Cyanide from Potassium Ferrocyanide
[quote]
It's Cu(CN)2, not CuCN2. Cu(CN)2 is unlikely to decompose to CuCN, as far as I know.[/quo ... |
23-6-2013 at 20:58
by: anomolous |
Silver and Copper Cyanide from Potassium Ferrocyanide
[quote]
The only role for the SO2 that I can think of is the reduction of cupric to cuprous catio ... |
23-6-2013 at 11:21
by: anomolous |
Silver and Copper Cyanide from Potassium Ferrocyanide
KCN, NaCN, and pretty much any other cyanide is hard to find in the US. Methods used to make these ... |
23-6-2013 at 00:43
by: anomolous |
Sodium ethoxide with NaOH and ethanol
Thanks, Dr Bob. The sodium ethoxide salts have been stored in a vacuum desiccator over CaCl, so they ... |
16-6-2013 at 21:51
by: anomolous |
Sodium ethoxide with NaOH and ethanol
Quick question. I precipitated sodium ethoxide salts per US patent 1978647 and was wondering how eas ... |
13-6-2013 at 20:47
by: anomolous |
Nitroethane from ethylsulfate, Desseigne variation.
Experimental 1: 300 mL of 96% H2SO4 was carefully added to 600 mL of ~95% ethyl alcohol in a 1000 mL ... |
2-4-2013 at 11:41
by: anomolous |
Nitroalkane syntheses ?
Experimental 1: 300 mL of 96% H2SO4 was carefully added to 600 mL of ~95% ethyl alcohol in a 1000 mL ... |
2-4-2013 at 11:40
by: anomolous |
Nitroalkane syntheses ?
So this is how information gets buried under tons of misinformation and unrelated dialog. Does anyon ... |
2-4-2013 at 11:37
by: anomolous |
Lab Prep of Diethyl Sulfate
I look forward to hearing any results. Proper equipment is a must if one even considers this reactio ... |
2-4-2013 at 11:05
by: anomolous |
Nitroalkane syntheses ?
I tried the reaction of 2-bromoproprionic acid with sodium nitrite in DMSO again. This time I vacuum ... |
30-3-2013 at 21:04
by: anomolous |
Lab Prep of Diethyl Sulfate
Thanks for your concern. I am aware of the risks in dealing with this substance and am taking the ne ... |
30-3-2013 at 21:01
by: anomolous |
Nitroethane from ethylsulfate, Desseigne variation.
Ah, thanks. I did try to neutralize with only Na2CO3 and did get some nitroethane but, you're right, ... |
30-3-2013 at 20:56
by: anomolous |
Nitroalkane syntheses ?
Destructive Distillation of 2-bromoproprionic acid
120 mL of K2CO3 sol. (pH 11) was poured into a ... |
27-3-2013 at 15:19
by: anomolous |
Nitroethane from ethylsulfate, Desseigne variation.
Can someone explain why Antoncho first neutralized the ethylsulfate with Lime and then with sodium c ... |
24-3-2013 at 10:24
by: anomolous |
Nitroalkane syntheses ?
Another semi-failed attempt:
10 g magnesium methoxide in 50 mL of DMSO, followed by 17 g 2-bromop ... |
24-3-2013 at 08:18
by: anomolous |
Nitroalkane syntheses ?
The reason I was attracted to this route was its apparent simplicity. I may try vacuum distilling in ... |
20-3-2013 at 22:44
by: anomolous |
Nitroethane from 2-Bromoproprionic acid
I'm not sure if I should have started a new thread or not. If so, I apologize.
Of the many synth ... |
17-3-2013 at 17:16
by: anomolous |
Diethyl Sulfate via Vacuum Distillation of Ethyl Sulfuric Acid
I know this is an old thread but I wanted to post my experience to save others, who might be conside ... |
12-3-2013 at 15:11
by: anomolous |
