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Removing sodium from a solution
Hi all,

Long time reader seldom poster here looking for a little advice.

I have a solution t ...
11-5-2015 at 09:36
by: atomicfire
Interesting and colorful coordination chemistry with ethylene diamine
How might one obtain some ethylene diamine?
11-9-2013 at 12:44
by: atomicfire
Any simple alternatives to vacuum pumps?
I use the compressor from an old mini fridge. I had a local heating and cooling place take the cool ...
12-12-2012 at 09:08
by: atomicfire
Magnesium Carbonate
Hi All,

I've got a question regarding magnesium carbonate and something called magnesium hydroxid ...
16-12-2011 at 05:50
by: atomicfire
Heating Mantle Problem
Update:

After a little investigation, the resistance of the bottom circuit of this mantle (it has ...
4-11-2011 at 08:51
by: atomicfire
Heating Mantle Problem
A porcelain crucible was used as the vessel and it was in contact with the mantle, although the cruc ...
2-11-2011 at 10:53
by: atomicfire
Heating Mantle Problem
Hey All,

I have a mantle from glas-col that the fiber lining in the rounded section became brittl ...
2-11-2011 at 05:28
by: atomicfire
Capsaicin extraction and isolation
Has anyone tried an extraction recently? I think I am going to try using Habaneros and doing an ext ...
9-10-2011 at 11:02
by: atomicfire
Thermite problem
I've used a 7/3 ratio (700g iron powder and 300g aluminum) and I get pretty molten ironglobs out of ...
9-9-2011 at 08:34
by: atomicfire
Potassium Persulfate Oxidizer
Great Information. Thank You!

I was originally only interested in if this oxidizer would even wo ...
8-7-2011 at 06:38
by: atomicfire
Potassium Persulfate Oxidizer
Thank you for the information, but I decided the best course of action was to experiment on my own. ...
6-7-2011 at 19:28
by: atomicfire
Potassium Persulfate Oxidizer
Being the season of fireworks and explosives, seeing some got me thinking of some good old flash pow ...
6-7-2011 at 05:02
by: atomicfire
aniline derivatives
Yeah, I don't think I can get bromine for that reaction.
7-6-2011 at 11:16
by: atomicfire
aniline derivatives
My goal is to synthesize anthranilic acid.

So, if one were to start with benzoic acid could one ...
7-6-2011 at 10:56
by: atomicfire
aniline derivatives
Could one convert the hydroxyl to a carboxilic acid?

And also, wouldn't the nitrosation occur at ...
7-6-2011 at 09:38
by: atomicfire
aniline derivatives
I am searching for a method to add a hydroxyl group in the ortho position on aniline. Does anyone k ...
7-6-2011 at 09:20
by: atomicfire
Vacuum Oven and Thermocouple
My thermodynamics teacher would flip if he saw this.

I get it now, thanks. Just needed a little ...
23-5-2011 at 10:14
by: atomicfire
Vacuum Oven and Thermocouple
This may seem like an odd question but in a vacuum oven, how does the thermocouple measure the tempe ...
23-5-2011 at 08:19
by: atomicfire
diazotization
What is the mechanism for such a reaction?
3-5-2011 at 07:48
by: atomicfire
diazotization
Is it possible to run a diazotization directly from a nitroso group?

Or how would one reduce it t ...
3-5-2011 at 06:45
by: atomicfire
Silver Azide
Can someone point me to some more info on Silver Azide?
28-4-2011 at 04:31
by: atomicfire
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
I've decided to test out this cell but I have a question.

I dissolved the ammonium sulfate in the ...
22-4-2011 at 04:16
by: atomicfire
Why does alcohol taste bad?
Taste, in my opinion, is completely subjective. What 'tastes' good to one may not 'taste' good to a ...
18-4-2011 at 11:49
by: atomicfire
Preparation of anthranilic acid
What is the reaction between phthalic anhydride and urea? Under what conditions does this occur?
18-4-2011 at 11:33
by: atomicfire
cleaning glass frit
From Adams & Chittenden Scientific:

"Fritted discs are made by heating glass particles or fib ...
6-4-2011 at 11:48
by: atomicfire
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