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Are dry solvents and inert atmo necessary? (NaBHOAc3 red amin))
I'm still new to synthesis, 2nd year grad student with one focus on synthesis. Now we always do stuf ...
22-9-2011 at 17:24
by: chemchemical
Middle Man/company to buy chemicals from? Starting a business?
I know this will probably get flagged but I do not yet have the ability to register a company in ord ...
27-2-2011 at 00:10
by: chemchemical
Computer in Lab protection
So i wanna start bringing my netbook into the lab with me (organic) but I'm worried about spills, sp ...
17-3-2010 at 07:24
by: chemchemical
Which is the better pump?
Yes, I would like to keep both but at the moment I could use the space and money, plus I dont really ...
14-2-2010 at 14:24
by: chemchemical
Which is the better pump?
I bought a vacuum pump not too long ago and just recently I came across a pump that was being thrown ...
13-2-2010 at 16:05
by: chemchemical
beginner question in regards to filtering
[rquote=169132&tid=13231&author=smuv]Take a fritted glass funnel, fill it with silica, the a ...
4-2-2010 at 15:26
by: chemchemical
sciencelab .com
Yes, do not order from them. I actually got a refund after calling about 5 times, but they only refu ...
4-2-2010 at 14:14
by: chemchemical
Nitrogen cylinder, welding experience required?
If you are looking to do a few inert reactions and don't need the amount in a tank, I would like to ...
27-9-2009 at 13:36
by: chemchemical
what can i coat the inside of my homemade fumehood with?
I have been thinking of a fume hood for awhile now and I personally would use a teflon or HDPE sheet ...
18-9-2009 at 21:55
by: chemchemical
Careers in chemistry
This sounds like me when I started undergrad. I ended up chosing the chemistry route and am going fo ...
18-9-2009 at 21:44
by: chemchemical
Computer lab/notebook program? Who takes notes on the computer?
[rquote=159500&tid=12640&author=daragh8008]That would great app for an itouch or iphone. Par ...
9-8-2009 at 19:06
by: chemchemical
Computer lab/notebook program? Who takes notes on the computer?
So I am trying to push our lab to use more technology and I would like to use my computer to take no ...
6-8-2009 at 06:11
by: chemchemical
making a quaternary salt from secondary amine?
Posted below is the link to the paper on the double N-methylation of a piperine derivative, I posted ...
6-4-2009 at 10:42
by: chemchemical
PEA and mek -> NPP?
I thought this article sounds interesting as a possible starting point to making NPP from PEA, unfor ...
14-3-2009 at 09:21
by: chemchemical
making a quaternary salt from secondary amine?
[quote][i]Originally posted by Nicodem[/i]
N,N-Dimethyl-3-chloropiperidinium salts, regardless of t ...
19-11-2008 at 17:15
by: chemchemical
methanesulfonic acid
[quote][i]Originally posted by Nicodem[/i]
It is only you that claim the methanesulfonic or toluene ...
19-11-2008 at 16:22
by: chemchemical
making a quaternary salt from secondary amine?
[quote][i]Originally posted by chemchemical[/i]
Well I'm trying to make a quaternary salt of a pipe ...
14-11-2008 at 16:15
by: chemchemical
making a quaternary salt from secondary amine?
[quote][i]Originally posted by chemrox[/i]
Please post that paper![/quote]

Here is the paper on ...
14-11-2008 at 16:03
by: chemchemical
making a quaternary salt from secondary amine?
[quote][i]Originally posted by Nicodem[/i]
Huh!?
[/quote]

Alright, well a little searching and ...
14-11-2008 at 16:00
by: chemchemical
making a quaternary salt from secondary amine?
I'm not trying to do a hoffman elimination.

chemrox: this is what confused me about the reaction ...
9-11-2008 at 18:25
by: chemchemical
making a quaternary salt from secondary amine?
Well I'm trying to make a quaternary salt of a piperidine-like compound to use as a leaving group in ...
7-11-2008 at 12:09
by: chemchemical
Manganese dioxide- make or buy?
I was going to use it to oxidize a hyroxy to ketone.

I read the other threads but it was about ob ...
18-10-2008 at 08:54
by: chemchemical
Manganese dioxide- make or buy?
I was thinking of using Manganese dioxide in a reaction, however I heard that it needs to be "activa ...
17-10-2008 at 18:02
by: chemchemical
Converting to the hydrochloric salt for storage?
sounds good, but it would still be possible to convert to the HCl salt with the acid, have it dissol ...
31-8-2008 at 08:57
by: chemchemical
Converting to the hydrochloric salt for storage?
Ok, so the last process in a synthesis is the conversion of the product to its HCl salt. They dissol ...
24-8-2008 at 17:07
by: chemchemical
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