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Potassium Permanganate Standard
Just used permanganate solution (standardised with potassium oxalate) to titrate an iron oxalate com ... |
28-8-2024 at 21:44
by: greenlight |
HMX via nitrolysis of DPT
@Denny, I agree, the worst you get is a yellow stain on your skin that peels off a few days later as ... |
12-8-2024 at 10:38
by: greenlight |
Short question / quick answer - Thread
The reason for trying to achieve the more granular crystals was for preparing plastic explosive whic ... |
12-8-2024 at 10:29
by: greenlight |
HMX via nitrolysis of DPT
I have never measured the specific gravity of the distilled and purged acids. I have just trusted t ... |
8-8-2024 at 09:11
by: greenlight |
Short question / quick answer - Thread
I have read that ETN is quite finnicky with wildly varying yields when multiple individuals follow ... |
8-8-2024 at 08:57
by: greenlight |
HMX via nitrolysis of DPT
[rquote=694544&tid=156126&author=ManyInterests]This thread is interesting because I also hav ... |
7-8-2024 at 08:42
by: greenlight |
Short question / quick answer - Thread
[rquote=694506&tid=26572&author=UndermineBriarEverglade]
[*]Is there a way to gauge nitrati ... |
7-8-2024 at 08:10
by: greenlight |
HMX via nitrolysis of DPT
That is a very interesting read with some thorough experimentation included.
At the time this thr ... |
5-8-2024 at 10:41
by: greenlight |
HMX via nitrolysis of DPT
Hello fellow EM chemists,
I am revisiting this method of HMX synthesis for two reasons:
1. T ... |
4-8-2024 at 06:34
by: greenlight |
short question about colored smoke bombs
The solvent dyes are the same ones used by the military and are pretty safe. I think the rhodamine ... |
3-8-2024 at 19:13
by: greenlight |
short question about colored smoke bombs
Fery is correct, you need a organic dye ( many are available on ebay if you search smoke dye like so ... |
3-8-2024 at 09:57
by: greenlight |
Chemistry behind RDX
[rquote=694201&tid=150602&author=DennyDevHE77][rquote=694183&tid=150602&author=green ... |
16-7-2024 at 06:07
by: greenlight |
Chemistry behind RDX
When I have made RDX I have always performed the nitrolysis then after addition is complete, allow i ... |
13-7-2024 at 10:10
by: greenlight |
Chemistry behind RDX
[rquote=693924&tid=150602&author=ManyInterests][rquote=693912&tid=150602&author=gree ... |
9-7-2024 at 10:55
by: greenlight |
LL8 from Dr. Liptakov
[rquote=694033&tid=158259&author=Laboratory of Liptakov]Just a due to sesitivity and unstabi ... |
9-7-2024 at 10:42
by: greenlight |
Rubidium Chlorate
Pretty cool stuff
You can use a methylene blue test for presence of perchlorate if you have, a ... |
9-7-2024 at 10:20
by: greenlight |
Chemistry behind RDX
[rquote=693905&tid=150602&author=ManyInterests]Decided to bump this up since I have been wor ... |
30-6-2024 at 18:59
by: greenlight |
Acetic anhydride preparation
[rquote=693492&tid=9&author=Keras]So today I've tried AcOH in DMSO + phosphorus pentoxide.
... |
30-6-2024 at 09:30
by: greenlight |
Can a perchlorate cell go wrong?
Great sign, you got perchlorate
It's always difficult with the perc cell because the product do ... |
29-6-2024 at 19:44
by: greenlight |
Separating Toluene from N-Butyl Acetate
Its not really a complex mixture, you have a difference in boiling point of 16°C. The 300mm vigreu ... |
29-6-2024 at 19:20
by: greenlight |
Can a perchlorate cell go wrong?
Have you done a test for the presence of perchlorate. I believe methylene blue was the one to use a ... |
29-6-2024 at 10:43
by: greenlight |
Separating Toluene from N-Butyl Acetate
You could use the allihn as a column without water circulating through it and pack it with broken gl ... |
29-6-2024 at 10:16
by: greenlight |
Separating Toluene from N-Butyl Acetate
How long is your column?
You could pack it with broken glass pieces for extra surface area for co ... |
29-6-2024 at 06:24
by: greenlight |
Nitric acid from calcium nitrate
You could also convert the calcium nitrate to potassium nitrate with potassium chloride if that's ea ... |
15-6-2024 at 09:33
by: greenlight |
Det cap questions: e-match nichrome, selecting a primary
I'm still a fan of aluminium cased caps filled with 700mg recrystallised, pressed PETN base charge, ... |
15-6-2024 at 09:24
by: greenlight |
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