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1-bromo-2-ethylhexane normal pressure distillation?
[rquote=641565&tid=155872&author=Fery]https://www.lookchem.com/2-Ethylhexyl-bromide/
190,8 ... |
27-7-2020 at 11:18
by: michalJenco |
1-bromo-2-ethylhexane normal pressure distillation?
Hi fellow chemist.
I am planning on making [url=https://www.sigmaaldrich.com/catalog/product/ALDR ... |
27-7-2020 at 09:25
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
After some time I have an update.
I followed [url=https://www.tandfonline.com/doi/abs/10.1080/003 ... |
2-7-2020 at 11:50
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
I did a melting point test in salty water (stopped at 105 °C) and my product didn't melt. Not sure ... |
18-6-2020 at 10:38
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
This also makes me wonder about what I actually made when I did this procedure with phenol and 2- an ... |
16-6-2020 at 16:08
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
Hmm that is worrying. I didn't do a m.p. test on the bottled product but it was liquid in the reacti ... |
16-6-2020 at 12:23
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638482&tid=155586&author=CuReUS][rquote=638383&tid=155586&author=Cou]
but I ... |
16-6-2020 at 09:59
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638475&tid=155586&author=Cou]What does 2,2'-oxydibenzoic acid smell like?[/rquote]
... |
16-6-2020 at 09:54
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638464&tid=155586&author=Cou][rquote=638384&tid=155586&author=Sigmatropic]If ... |
15-6-2020 at 15:35
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638441&tid=155586&author=Boffis]I would be interested in the procedure you used to p ... |
15-6-2020 at 14:41
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638384&tid=155586&author=Sigmatropic]If you could dehydrate it to the cyclic anhydri ... |
15-6-2020 at 13:43
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638383&tid=155586&author=Cou][img]https://i.imgur.com/BjRkctj.png[/img]
Interesti ... |
15-6-2020 at 13:40
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638379&tid=155586&author=UC235]You're trying to make an 11-membered ring which is re ... |
15-6-2020 at 13:25
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638389&tid=155586&author=Pumukli]Have you checked the price of the acid what you've ... |
15-6-2020 at 10:51
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
I did condensation of salicylic acid with o-chlorobenzoic acid in very basic very hot water.
Edit ... |
14-6-2020 at 09:30
by: michalJenco |
Cyclic diester from 2,2'-oxydibenzoic acid?
Hi fellow chemists.
I recently made [url=https://www.sigmaaldrich.com/catalog/product/aldrich/s53 ... |
14-6-2020 at 09:14
by: michalJenco |
Synthesis of diethyl diethylmalonate
Btw your advice to add KI as a "catalyst" is exactly what I've been thinking about myself but couldn ... |
6-6-2020 at 11:42
by: michalJenco |
Synthesis of diethyl diethylmalonate
I linked [url=http://www.orgsyn.org/demo.aspx?prep=CV1P0250]this[/url] procedure in a previous post ... |
6-6-2020 at 11:35
by: michalJenco |
Synthesis of diethyl diethylmalonate
From what I've seen alkyl bromides are used. But even if not, I haven't even got to that step becaus ... |
6-6-2020 at 11:20
by: michalJenco |
Synthesis of diethyl diethylmalonate
This synthesis is absolute nonsense, even after adding a few milliliters of dried ester to ethoxide ... |
6-6-2020 at 10:30
by: michalJenco |
Synthesis of diethyl diethylmalonate
I bought it just a few weeks ago and the label says >99%. But I guess I'll throw in some sieves a ... |
6-6-2020 at 10:01
by: michalJenco |
Synthesis of diethyl diethylmalonate
Ok I repeated the experiment and added diethyl malonate to sodium ethoxide slowly at under 50°C and ... |
6-6-2020 at 09:25
by: michalJenco |
Synthesis of diethyl diethylmalonate
After reading further I found a synthesis of diethyl butylmalonate where they specify to add the die ... |
5-6-2020 at 11:33
by: michalJenco |
Synthesis of diethyl diethylmalonate
Hi fellow chemists.
I am currently running a synthesis of [url=https://www.sigmaaldrich.com/catal ... |
5-6-2020 at 11:10
by: michalJenco |
Procedure for Coumarin - different product, what is it?
Still nobody has any idea? |
9-5-2020 at 14:12
by: michalJenco |
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