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Toluene to Aniline path
If you want to use aniline for further reactions, and it is not an end-goal, a much easier route is ... |
17-7-2018 at 08:30
by: myristicinaldehyde |
Thiocyanation of Vanillin using Cu(ii) Advice
An update: I prepared a putative Br2 solution using TCCA in glacial acetic acid, which was then filt ... |
10-7-2018 at 12:03
by: myristicinaldehyde |
Thiocyanation of Vanillin using Cu(ii) Advice
I tried 2 thiocyanations, a Tetrahedron Letters article claimed I2/MeOH would work (it did not) and ... |
1-7-2018 at 07:51
by: myristicinaldehyde |
Thiocyanation of Vanillin using Cu(ii) Advice
A long time ago I came across this interesting procedure in Shulgin:
[quote]
o an ice cold and w ... |
13-6-2018 at 13:35
by: myristicinaldehyde |
Preparation of 5-hydroxyvanillin
Thank you! I am waiting for more vanillin to arrive, so I can try using bromide instead of iodide &a ... |
13-6-2018 at 08:05
by: myristicinaldehyde |
Preparation of 5-hydroxyvanillin
Attached is my write-up. Other than marveling at my fantastic ineptitude in the lab, any comments wo ... |
27-5-2018 at 13:14
by: myristicinaldehyde |
Advice with Hydroxyvanillin?
(Take a wild guess at what it will be used for)
I think I finally arrived at hydroxyvanillin, aft ... |
25-4-2018 at 16:24
by: myristicinaldehyde |
The nitration of styrenes by nitric acid in dichloromethane
[url=http://www.libgen.io]Use Library Genesis. [/url] |
25-4-2018 at 12:28
by: myristicinaldehyde |
Nitration of Vanillin with KNO3/H2SO4 in Acetic Acid
[rquote=513308&tid=81759&author=Boffis]Yes, nice work. I suspect that the nitro group enters ... |
6-4-2018 at 11:01
by: myristicinaldehyde |
Nitration of Vanillin with KNO3/H2SO4 in Acetic Acid
Nitration of Vanillin with KNO3/H2SO4 in Acetic Acid
Materials:
Vanillin (25mmol -> 3.8g)
KN ... |
5-4-2018 at 11:55
by: myristicinaldehyde |
Experiments with Vanillin and Ethyl Vanillin Ideas
[rquote=509892&tid=81023&author=Vicarious3rdEye2]That's what fascinates me though so much ab ... |
8-3-2018 at 13:10
by: myristicinaldehyde |
Bromovanillin Workup?
I found a few procedures that claimed high yielding and quick bromination of phenols and phenol ethe ... |
4-2-2018 at 11:28
by: myristicinaldehyde |
Preparation of Acetaldehyde
https://www.sciencemadness.org/whisper/viewthread.php?tid=55
utfse |
24-12-2017 at 10:16
by: myristicinaldehyde |
Xysyl chloride as a protecting group? Substitute for Tosyl Chloride.
This might help you http://orgsyn.org/demo.aspx?prep=CV7P0508
Chlorination of a sulfonic acid wit ... |
27-11-2017 at 11:41
by: myristicinaldehyde |
Help recrystalizing dimethylbenzenesulfonic acid
It ended up crystalizing by itself when I took it *out* of the freezer. Hmmm. |
25-11-2017 at 12:56
by: myristicinaldehyde |
Help recrystalizing dimethylbenzenesulfonic acid
I followed the following procedure from Vogel's 5 th edition. It worked almost exactly as described, ... |
25-11-2017 at 04:47
by: myristicinaldehyde |
Sulforaphane
Some good posts in this thread:
http://www.sciencemadness.org/talk/viewthread.php?tid=75864
|
15-11-2017 at 13:35
by: myristicinaldehyde |
Fisher Scientific & Restricted Chemicals
As an update on what, exactly, I wanted to buy (I wrote a nice, long post but then lost it)
Many ... |
28-10-2017 at 11:13
by: myristicinaldehyde |
Synthesis of dopamine from catechol
This is an interesting alternative to dopamine, via a pummerer rearrangement and subsequent reductio ... |
24-10-2017 at 02:58
by: myristicinaldehyde |
Could Greed end research gate?
Well, thank God for Russian servers! In my opinion, the Elsevier model is deeply unethical, and so i ... |
12-10-2017 at 12:29
by: myristicinaldehyde |
Fisher Scientific & Restricted Chemicals
Mario is still active- I'll send him an email, but I'd rather stay local- the shipping from PL to th ... |
9-10-2017 at 09:29
by: myristicinaldehyde |
Fisher Scientific & Restricted Chemicals
While the common wisdom is that Fisher Scientific does not sell to individuals, this is not complete ... |
9-10-2017 at 07:13
by: myristicinaldehyde |
Lithium Metal for sale
Price? |
28-9-2017 at 13:15
by: myristicinaldehyde |
The "WTF did I just make?" thread
I have something mildly interesting.
A solution of copper sulfate and dilute sulfuric acid, when ... |
1-9-2017 at 10:39
by: myristicinaldehyde |
The Short Questions Thread (4)
So I made some isopropyl bromide (9.0g total). My next planned step is to try to see if I can alkyla ... |
11-8-2017 at 15:34
by: myristicinaldehyde |
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