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Oxidation of styrene to phenylacetaldehyde
Works in acetone over silica gel in high yield. Forgot the name of the paper though it should be eas ...
15-7-2018 at 10:17
by: notoxicshit
Phenylpropanones (P2P) from anilines
I can buy mapp gas in germany easily. Who wants some?
14-6-2018 at 13:43
by: notoxicshit
amino acid + O² = a-nitro acid + formaldehyde - CO² = nitroalkene
What is it that is wrong with this thread?

The point is:
I really am motivated to experiment on ...
23-4-2018 at 12:35
by: notoxicshit
amino acid + O² = a-nitro acid + formaldehyde - CO² = nitroalkene
Yeah no problem really, I'm fine with DMDO since acetone and oxone are both cheap. Also not a proble ...
10-4-2018 at 03:43
by: notoxicshit
amino acid + O² = a-nitro acid + formaldehyde - CO² = nitroalkene
Its not that I dont like your suggestion, its that I just dont have the reagents.
As I said, I wil ...
9-4-2018 at 08:02
by: notoxicshit
amino acid + O² = a-nitro acid + formaldehyde - CO² = nitroalkene
I first need to understand why you proposed an alternative. What thought lies behind that?
Like I s ...
9-4-2018 at 05:25
by: notoxicshit
amino acid + O² = a-nitro acid + formaldehyde - CO² = nitroalkene
I want to research organic reduction methods, from nickel urushibara, over Al/Ga & Al/Cu to self ...
8-4-2018 at 05:25
by: notoxicshit
First attempt Grignard since Ochem II cyclopentyl bromide
I dont understand what leads you to believe that there is a problem with your reaction besides too l ...
4-4-2018 at 06:21
by: notoxicshit
Alkali nitrite salt (home production, purification via esterification)
I am german and I fear the Zoll. I dont want any attention. Of course its not exactly illegal to buy ...
5-3-2018 at 04:19
by: notoxicshit
Alkali nitrite salt (home production, purification via esterification)
It wouldnt be a problem to source some impure nitrate for fertilizing purposes or HNO3.

I would u ...
4-3-2018 at 03:33
by: notoxicshit
Alkali nitrite salt (home production, purification via esterification)
Well fuck me sideways, this is amazing.

Not even and iodide involved


This is exactly what I ...
3-3-2018 at 15:26
by: notoxicshit
Alkali nitrite salt (home production, purification via esterification)
Iodine salts are not too expensive for me, especially when the product is more valuable.

It is a ...
3-3-2018 at 05:39
by: notoxicshit
Alkali nitrite salt (home production, purification via esterification)
So the more developed parts of mainland europe do in parts have the problem that "toxic" chemicals a ...
2-3-2018 at 12:13
by: notoxicshit
Preparation of aluminium triethoxide without mercury?
Treating the aluminium with gallinstan should work and most likely make the iodine not necessary.
A ...
2-8-2017 at 03:17
by: notoxicshit
Gallium-based aluminum reducing reagents, free to USA members who do a writeup
Very interesting and Id be glad to help but I am european.

Planned to do further experimentation ...
19-7-2017 at 04:24
by: notoxicshit
Photophthalimidation of unactivated alkenes
So I have detected a facial uv radiation apparatus for achieving a tan.
It seems to have a filteri ...
18-7-2017 at 10:25
by: notoxicshit
Photophthalimidation of unactivated alkenes
What I need to know is, why is just "pyrex" mentioned as the kind of glas they use? Does that indica ...
17-7-2017 at 16:19
by: notoxicshit
Photophthalimidation of unactivated alkenes
I had been looking up some stuff about phthalimide and phthalic anhydride, when I came across a pape ...
16-7-2017 at 16:18
by: notoxicshit
"Novel Method of Reducing Ketones Using Sodium Hydroxide in Isopropanol"
Excuse the double post, but since all of my questions have been ignored, here are the most important ...
26-2-2017 at 10:22
by: notoxicshit
Refractometer Range
I'm at the point where I need to buy a refractometer.
At the moment I am seriously tight with money ...
26-2-2017 at 10:13
by: notoxicshit
"Novel Method of Reducing Ketones Using Sodium Hydroxide in Isopropanol"
Works, gives a product that can be dehydrated with KHSO4.
Did this because the bps of product and s ...
26-2-2017 at 09:50
by: notoxicshit
"Novel Method of Reducing Ketones Using Sodium Hydroxide in Isopropanol"
Well the reflux doesn't serve any purpose other than maximizing the reaction temperature to the BP o ...
24-2-2017 at 09:05
by: notoxicshit
"Novel Method of Reducing Ketones Using Sodium Hydroxide in Isopropanol"
Other points I'd like to hear opinions about : how moisture sensitive should the reaction be?

Theo ...
23-2-2017 at 13:48
by: notoxicshit
"Novel Method of Reducing Ketones Using Sodium Hydroxide in Isopropanol"
Would you be so kind to retype your answer? I'm interested in anything people have to say.

I miss ...
23-2-2017 at 13:42
by: notoxicshit
"Novel Method of Reducing Ketones Using Sodium Hydroxide in Isopropanol"
I'd like to discuss a reaction I stumbled upon. It's from 2010, from an american university.

I at ...
23-2-2017 at 12:01
by: notoxicshit
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