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preparation of succinic anhydride from succinic acid (using a Dean-Stark trap) Nice work!
Apparently, succinic anhydride can also be made by thermal dehydration of neat succinic ... |
25-1-2026 at 12:18 by: oberkarteufel |
6- Benzyl Azulene synthesis Does this procedure also work with other pyridines? The regular one, the ones with alkyl, nitro, ami ... |
16-1-2026 at 21:58 by: oberkarteufel |
Propylene (oxide) synthesis An excerpt from Org. Synth. 1988, 66, 160 (DOI: 10.15227/orgsyn.066.0160) [b]"(R)-ALKYLOXIRANES OF H ... |
3-1-2026 at 03:28 by: oberkarteufel |
seperation ketones I'd say that the minimal difference of boiling points for simple distillation is 50 degrees.
For 2 ... |
12-10-2025 at 19:46 by: oberkarteufel |
Embarrassing question about Grignard reaction [rquote=703627&tid=161242&author=chempyre235]So, it sounds like you'd get ethyl lactate, or ... |
12-10-2025 at 10:25 by: oberkarteufel |
Embarrassing question about Grignard reaction Since it bothered me this much, I dug deeper than the dwarves of Khazad-dûm and I'll share the answ ... |
9-10-2025 at 21:11 by: oberkarteufel |
Embarrassing question about Grignard reaction Thank you for the answers. Well, I'll keep digging, maybe something pops out. |
17-8-2025 at 23:31 by: oberkarteufel |
Embarrassing question about Grignard reaction Hi. Everyone knows Grignard reaction, many know other reactions of Grignard reagents.
As you know, ... |
14-8-2025 at 06:44 by: oberkarteufel |
DIY homemade hydrothermal crystallization device @Twospoons - thanks for the info about those heating cables, I'll look it up.
@Admagistr - not re ... |
10-2-2023 at 09:15 by: oberkarteufel |
DIY homemade hydrothermal crystallization device @Mateo_swe - thanks for the encouragement, but as I noted in the first post - my heating system does ... |
9-2-2023 at 10:34 by: oberkarteufel |
DIY homemade hydrothermal crystallization device "O szlachetnych kryształach" ("On the precious crystals") Krzysztof Błaszkowski, Warsaw 1987, ISBN ... |
9-2-2023 at 03:40 by: oberkarteufel |
Making rubies using microwave [rquote=667110&tid=158046&author=Admagistr] I used a CaO to capture the MoO3 vapor. [/rquote ... |
29-1-2023 at 02:40 by: oberkarteufel |
A dilemma with molasses and pH control Hello CocoMoco, I know it's probably too late, but I would like to know something about your process ... |
27-8-2020 at 02:50 by: oberkarteufel |
Uranyl acetate to nitrate A little update with a couple conclusions.
3% H2O2 works fine for precipitating uranyl peroxide. ... |
27-8-2020 at 02:03 by: oberkarteufel |
Uranyl acetate to nitrate @Heptylene - thank you for the information. I might try with 3% first, as it is much less hassle to ... |
9-7-2020 at 00:04 by: oberkarteufel |
Uranyl acetate to nitrate Kindly thank you for your answer. Your advice provides a good insight, it can be seen that you've re ... |
8-7-2020 at 00:13 by: oberkarteufel |
Uranyl acetate to nitrate Hello!
Some time ago I got interested in an old photography technique called uranotype. For now, t ... |
7-7-2020 at 02:29 by: oberkarteufel |
Gold extraction attempt @diddi - I know, and I did this only for fun, yyyyy educational purpose, of course 
@Sulaiman - ... |
4-12-2019 at 03:21 by: oberkarteufel |
Make Potassium (from versuchschemie.de) Yup, same paraffin oil from pharmacy, heating regime etc. IIRC Total time of heating (first for dryi ... |
4-12-2019 at 03:11 by: oberkarteufel |
Gold extraction attempt Ha, that's a nice amount, indeed 
Non-profit maybe, but highly educational and verily addictive, ... |
3-12-2019 at 12:31 by: oberkarteufel |
Gold extraction attempt So one day I decided I have too much money ([i]yeeeeaaah, sure[/i]) and I bought some 14k (583) gold ... |
3-12-2019 at 05:12 by: oberkarteufel |
Carry on with active metals... Some time ago I have tried the thermite-type reaction to produce some sodium.
Some notes for the on ... |
3-12-2019 at 04:28 by: oberkarteufel |
Success! Well, for longer I've been away from this topic than expected, but I'm back with some new results.
... |
3-12-2019 at 04:08 by: oberkarteufel |
sodium metal extraction - Nurdrage did it! Followed 12thealchemist's suggestion from https://www.sciencemadness.org/whisper/viewthread.php?tid= ... |
16-6-2019 at 10:02 by: oberkarteufel |
sodium metal extraction - Nurdrage did it! In this topic it's an off-top, but I'll answer.
I'm leaning towards the opininon that menthol does ... |
16-6-2019 at 00:24 by: oberkarteufel |
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