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First yield of KClO3 from my cell
Sure, but getting an accurate measurement of volume would be difficult. An option would be to first ... |
1-7-2021 at 09:08
by: vanBassum |
First yield of KClO3 from my cell
Haha you are completely right about the caveman style. 
My cell is still comparable to the phot ... |
1-7-2021 at 08:33
by: vanBassum |
First yield of KClO3 from my cell
Oh, this thread has progressed significantly since I last logged-in.
I run my cell with and wi ... |
30-6-2021 at 10:08
by: vanBassum |
Measuring the perchlorate cell
Oh I think you missed the point, I am trying to create a PbO2 anode from my old MMO. There will prob ... |
11-2-2021 at 05:38
by: vanBassum |
Measuring the perchlorate cell
So, I am trying to create my own PbO2 anodes. I've used a dead MMO as cathode and 2 lead anodes on e ... |
10-2-2021 at 03:46
by: vanBassum |
Measuring the perchlorate cell
Yea I know, I let it run for a couple of days, then I do a fractional crystallization. The filtrate ... |
7-2-2021 at 11:08
by: vanBassum |
Measuring the perchlorate cell
Ohh I just destroyed another MMO, aaargh. Let it run for too long, I should program in a stop when t ... |
6-2-2021 at 04:31
by: vanBassum |
Measuring the perchlorate cell
I finished up the run yesterday. When testing with HCl it tests negative for chlorate, but the indig ... |
11-1-2021 at 03:01
by: vanBassum |
Casting busbars for a TSLD anode
Thanks for the warning, I won't take that chance. Although fixing the anode might be possible, I pre ... |
9-1-2021 at 12:08
by: vanBassum |
Casting busbars for a TSLD anode
Thanks for the tip, but I already bought some pure NaF. It was 25 euro for 500g so not to bad. I've ... |
9-1-2021 at 10:44
by: vanBassum |
Casting busbars for a TSLD anode
Aha, that makes sense. NaCl won't work then because of passivation. I'll just stop dicking around an ... |
9-1-2021 at 07:49
by: vanBassum |
Casting busbars for a TSLD anode
I am currently experimenting with electroplating copper on titanium. Thing is, I don't have any NaF. ... |
9-1-2021 at 06:50
by: vanBassum |
Measuring the perchlorate cell
Thanks for the information!
I am currently building a new MMO cell to replace the old one. When I ... |
9-1-2021 at 06:29
by: vanBassum |
Measuring the perchlorate cell
I just took a sample of the cell to which I added saturated KClO3 solution. A precipitate of KClO4 f ... |
8-1-2021 at 03:09
by: vanBassum |
Casting busbars for a TSLD anode
I have read about guys electroplating the top with copper. I didn't bother with it just used cable l ... |
8-1-2021 at 02:50
by: vanBassum |
Measuring the perchlorate cell
Good to know that my MMO can be used for a new purpose. I don't really trust the state the MMO was w ... |
7-1-2021 at 07:05
by: vanBassum |
Measuring the perchlorate cell
I just put the cell in a water bath, since the cell was already placed in a bucket this was quite an ... |
7-1-2021 at 06:34
by: vanBassum |
Measuring the perchlorate cell
Hello,
I have been playing around with a PbO2 perchlorate cell for a little while now. While doin ... |
6-1-2021 at 09:42
by: vanBassum |
Solubility of salts and their percipitation
A quick update: I changed my setup to 2 different cells. The first cell is a MMO for making sodium c ... |
6-10-2020 at 00:36
by: vanBassum |
Solubility of salts and their percipitation
That site is an absolute treasure! I stumbled across it ones before. First I will download the site ... |
28-9-2020 at 11:14
by: vanBassum |
Solubility of salts and their percipitation
Ah yes I've seen that video before that's a very nice setup, and I am a bit jealous of his glassware ... |
24-9-2020 at 01:54
by: vanBassum |
Solubility of salts and their percipitation
Hello,
Yes I am talking about sodium salts, because I have read that potassium salts are too inso ... |
23-9-2020 at 23:57
by: vanBassum |
Solubility of salts and their percipitation
Hello guys,
First of all, this question might be very simple but since I have no real background ... |
23-9-2020 at 08:30
by: vanBassum |
Simple exploding wire apparatus for nanopowders
Hello,
So I might be able to help you with this. I don't have an inert atmosphere but I can try t ... |
19-8-2020 at 06:52
by: vanBassum |
eU2A method for generating ammonia
Well....
It turns out it doesn't work with NaOH but it does with KOH.
Now I get the very recogni ... |
12-8-2020 at 02:25
by: vanBassum |
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