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Measuring the perchlorate cell
Oh I think you missed the point, I am trying to create a PbO2 anode from my old MMO. There will prob ...
11-2-2021 at 05:38
by: vanBassum
Measuring the perchlorate cell
So, I am trying to create my own PbO2 anodes. I've used a dead MMO as cathode and 2 lead anodes on e ...
10-2-2021 at 03:46
by: vanBassum
Measuring the perchlorate cell
Yea I know, I let it run for a couple of days, then I do a fractional crystallization. The filtrate ...
7-2-2021 at 11:08
by: vanBassum
Measuring the perchlorate cell
Ohh I just destroyed another MMO, aaargh. Let it run for too long, I should program in a stop when t ...
6-2-2021 at 04:31
by: vanBassum
Measuring the perchlorate cell
I finished up the run yesterday. When testing with HCl it tests negative for chlorate, but the indig ...
11-1-2021 at 03:01
by: vanBassum
Casting busbars for a TSLD anode
Thanks for the warning, I won't take that chance. Although fixing the anode might be possible, I pre ...
9-1-2021 at 12:08
by: vanBassum
Casting busbars for a TSLD anode
Thanks for the tip, but I already bought some pure NaF. It was 25 euro for 500g so not to bad. I've ...
9-1-2021 at 10:44
by: vanBassum
Casting busbars for a TSLD anode
Aha, that makes sense. NaCl won't work then because of passivation. I'll just stop dicking around an ...
9-1-2021 at 07:49
by: vanBassum
Casting busbars for a TSLD anode
I am currently experimenting with electroplating copper on titanium. Thing is, I don't have any NaF. ...
9-1-2021 at 06:50
by: vanBassum
Measuring the perchlorate cell
Thanks for the information!

I am currently building a new MMO cell to replace the old one. When I ...
9-1-2021 at 06:29
by: vanBassum
Measuring the perchlorate cell
I just took a sample of the cell to which I added saturated KClO3 solution. A precipitate of KClO4 f ...
8-1-2021 at 03:09
by: vanBassum
Casting busbars for a TSLD anode
I have read about guys electroplating the top with copper. I didn't bother with it just used cable l ...
8-1-2021 at 02:50
by: vanBassum
Measuring the perchlorate cell
Good to know that my MMO can be used for a new purpose. I don't really trust the state the MMO was w ...
7-1-2021 at 07:05
by: vanBassum
Measuring the perchlorate cell
I just put the cell in a water bath, since the cell was already placed in a bucket this was quite an ...
7-1-2021 at 06:34
by: vanBassum
Measuring the perchlorate cell
Hello,

I have been playing around with a PbO2 perchlorate cell for a little while now. While doin ...
6-1-2021 at 09:42
by: vanBassum
Solubility of salts and their percipitation
A quick update: I changed my setup to 2 different cells. The first cell is a MMO for making sodium c ...
6-10-2020 at 00:36
by: vanBassum
Solubility of salts and their percipitation
That site is an absolute treasure! I stumbled across it ones before. First I will download the site ...
28-9-2020 at 11:14
by: vanBassum
Solubility of salts and their percipitation
Ah yes I've seen that video before that's a very nice setup, and I am a bit jealous of his glassware ...
24-9-2020 at 01:54
by: vanBassum
Solubility of salts and their percipitation
Hello,

Yes I am talking about sodium salts, because I have read that potassium salts are too inso ...
23-9-2020 at 23:57
by: vanBassum
Solubility of salts and their percipitation
Hello guys,

First of all, this question might be very simple but since I have no real background ...
23-9-2020 at 08:30
by: vanBassum
Simple exploding wire apparatus for nanopowders
Hello,

So I might be able to help you with this. I don't have an inert atmosphere but I can try t ...
19-8-2020 at 06:52
by: vanBassum
eU2A method for generating ammonia
Well....

It turns out it doesn't work with NaOH but it does with KOH.
Now I get the very recogni ...
12-8-2020 at 02:25
by: vanBassum
eU2A method for generating ammonia
Hello,

I saw an electrolytical method of generating ammonia gas from urea somewhere in this threa ...
10-8-2020 at 05:33
by: vanBassum
KClO4 from heating NaClO3
Wow, I need a moment to let this information sink in. My theoretical chemistry knowledge isn't too s ...
6-4-2020 at 04:42
by: vanBassum
KClO3 cell continuous production
True, but for sodium its more of a pain.
I get around this problem by reusing the filtrate to top ...
23-3-2020 at 07:08
by: vanBassum
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