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Hydrochloric acid impurities, where do they come from?
I personally know a retired chemical engineer who worked for one of the major world-famous chemical ...
14-7-2019 at 18:07
by: wakatutu
Failure to make Chloroform - help
The process I've employed is generally to first make a bleach slushy - you pour off enough bleach fr ...
22-6-2019 at 18:49
by: wakatutu
methyl chloride from dimethyl sulfate
http://www.sciencemadness.org/talk/viewthread.php?tid=77162#pid515474
a detailed report on the acci ...
9-4-2019 at 00:18
by: wakatutu
Possible OTC, 'safe' methylating agents
https://images.homedepot-static.com/catalog/pdfImages/da/da1f572a-88f6-43c2-9ccc-fa511b4b4c1b.pdf
s ...
8-4-2019 at 22:54
by: wakatutu
methyl chloride from dimethyl sulfate
Methyl Chloride unto itself is a nasty beast. It has all the same symptoms as methyl bromide and me ...
7-4-2019 at 17:20
by: wakatutu
Benzhydrol from Diphenhydramine
http://www.orgsyn.org/demo.aspx?prep=cv1p0090

Looks like benzophenone can be reduced using zinc a ...
19-1-2019 at 16:28
by: wakatutu
Unusual periodic table
https://en.wikipedia.org/wiki/Alternative_periodic_tables
I'm rather fond of Benfey's snail model
12-1-2019 at 23:05
by: wakatutu
Possible Hydrodehalogenation?
Thanks, AJKOER.

It makes sense that there would be an essentially electrochemical mechanism at ...
9-12-2018 at 21:20
by: wakatutu
Possible Hydrodehalogenation?
2Cu[sub]2[/sub]O + 2HCl + CH[sub]2[/sub]Cl[sub]2[/sub] ---->

2CuO + 2CuCl + H[sub]2[/sub] + CH ...
7-12-2018 at 00:11
by: wakatutu
making ethylene
@UC235 - regarding the dehalogenation of vicinal dihalides using NaI in a polar solvent - do you thi ...
6-12-2018 at 23:54
by: wakatutu
Filtering Hydroxide solution
Hi everybody!

I realize this is probably a topic already covered here, but using the search engin ...
10-6-2018 at 16:46
by: wakatutu
CuSO4, Bromides, Neurotoxic Gas (LONG POST)
There is a single aryl-methyl ether (aka a methoxy group on the benzene ring), at the 3 position of ...
25-4-2018 at 20:34
by: wakatutu
CuSO4, Bromides, Neurotoxic Gas (LONG POST)
Well, the world keeps turning and I keep mostly improving, as I hope all of you are as well!

I ...
24-4-2018 at 19:31
by: wakatutu
Synthesis of dopamine from catechol
Since people are asking about it, I have never seen a write up of an amateur successful with produci ...
11-11-2017 at 18:17
by: wakatutu
CuSO4, Bromides, Neurotoxic Gas (LONG POST)
Thanks for your responses. All of you have shared valuable knowledge, mostly in the form of forum p ...
17-10-2017 at 17:26
by: wakatutu
CuSO4, Bromides, Neurotoxic Gas (LONG POST)
I've certainly considered that stress was a factor but there was absolutely an underlying toxicity i ...
29-9-2017 at 13:50
by: wakatutu
CuSO4, Bromides, Neurotoxic Gas (LONG POST)
Short answer, yes, there was a ketone in contact with bromine, I think.

Long answer: these are hy ...
28-9-2017 at 20:52
by: wakatutu
CuSO4, Bromides, Neurotoxic Gas (LONG POST)
(continuing from above)

Here are the exact notes describing the problems at the time, when I seri ...
28-9-2017 at 15:25
by: wakatutu
CuSO4, Bromides, Neurotoxic Gas (LONG POST)
Well, this post is not going to be a fun one. Putting it in beginnings because I'm obviously not ve ...
28-9-2017 at 15:11
by: wakatutu
Br2 in DCM
Thank you again for your concern. The health effects of my bromine exposure have now worn off and I ...
13-4-2017 at 01:15
by: wakatutu
strangely smelling pepper compound?
are you sure it's not just piperidine?

The description of the smell tends toward piperinic acid, ...
13-4-2017 at 01:01
by: wakatutu
Br2 in DCM
I have concluded that I am allergic to bromine. Like I said, my associate was there as well and enc ...
24-2-2017 at 22:12
by: wakatutu
Br2 in DCM
Thanks for the responses!

I do not plan on working with this particular reaction mixture again. ...
23-2-2017 at 13:50
by: wakatutu
Br2 in DCM
Hello everyone! Long-time reader of the forum, I'll get to my introduction later on somewhere else. ...
23-2-2017 at 00:50
by: wakatutu

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