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Diethyl Ether - Illustrated Practical Guide
Nice work you've done here. |
17-3-2012 at 19:33
by: white rabbit |
Thoughts On Anodes
Buy the platinum anode and you're done. It saves 100's of hours of your precious time looking for al ... |
3-8-2010 at 17:40
by: white rabbit |
Condenser cooling
Hey thanks, Peach.
That polymer $hit seems to be highly soluble in water and cleaned up nicely.
... |
14-7-2010 at 18:08
by: white rabbit |
Thoughts On Anodes
You may have a good point there. That one electrode was never used as a anode. I have used thre ... |
22-6-2010 at 15:26
by: white rabbit |
Thoughts On Anodes
I will concede that platinum is indeed resistant but not impervious to electro/chemical attack ... |
21-6-2010 at 19:11
by: white rabbit |
Thoughts On Anodes
My point was simply, if the platinum is plating across, it is certainly not plating on the plat ... |
20-6-2010 at 09:51
by: white rabbit |
Thoughts On Anodes
[rquote=180387&tid=5050&author=hissingnoise][rquote=180324&tid=5050&author=white rab ... |
19-6-2010 at 16:42
by: white rabbit |
Thoughts On Anodes
Here is something that you probably don't come across too often.It appears to be a sodium chlorate c ... |
18-6-2010 at 13:48
by: white rabbit |
Thoughts On Anodes
@ Alexein/The electrodes were very reasonable, I think, at about $135 each including the shipping. I ... |
18-6-2010 at 13:30
by: white rabbit |
Thoughts On Anodes
I have found that the platinum clad niobium electrodes from Anomet work exceptionally well. After we ... |
15-6-2010 at 20:08
by: white rabbit |
Extract of Benzene thread
I have confirmed the good work others have done. I did not use anything in the retort for thermal co ... |
15-6-2010 at 18:50
by: white rabbit |
Condenser cooling
I've tried the coil in a bucket and it doesn't work as well. Modifications to window units are not a ... |
9-6-2010 at 15:14
by: white rabbit |
Condenser cooling
Thanks.
I have recently modified the design of my water cooler and it's a great improvement over ... |
8-6-2010 at 21:34
by: white rabbit |
Preparation of solid aluminium isopropoxide
I just left the N2 flowing about two bubbles per second and a CaCl2 guard at the top of the condense ... |
7-6-2010 at 14:11
by: white rabbit |
Preparation of solid aluminium isopropoxide
True! But I like the way they sit on the counter when I'm done and that one is really thick. |
4-6-2010 at 18:33
by: white rabbit |
Condenser cooling
I got most of my glassware on ebay. The large condenser retails for $1100 I got it for $250 |
4-6-2010 at 13:58
by: white rabbit |
Preparation of solid aluminium isopropoxide
The vacuum pump I used only got down to 10mm and molecular sieves with work just fine if you use eno ... |
4-6-2010 at 13:54
by: white rabbit |
Condenser cooling
Yeah,I believe its called "number 2"-009 sound system.
Btw,it's M1 property,not R1. |
27-5-2010 at 17:17
by: white rabbit |
Condenser cooling
Maybe :} |
27-5-2010 at 16:20
by: white rabbit |
Condenser cooling
Here is a jacketed Dimroth style condenser. The Dimroth coil is 8mm tubing and the tube down the cen ... |
27-5-2010 at 15:44
by: white rabbit |
Condenser cooling
[rquote=178623&tid=12367&author=azo]why in the hell would you want to go to that mutch troub ... |
26-5-2010 at 19:50
by: white rabbit |
Condenser cooling
Hey there mr.crow,
Here the tap water isn't very cold and it ain't cheap either. This is why I mad ... |
26-5-2010 at 17:29
by: white rabbit |
Condenser cooling
[rquote=175892&tid=12367&author=MagicJigPipe]To be fair it's probably not cheap to run a 500 ... |
26-5-2010 at 14:51
by: white rabbit |
Preparation of solid aluminium isopropoxide
Here are a few pics of the process
removal of excess water by NaOH
[file]10597[/file]
Disti ... |
26-5-2010 at 14:42
by: white rabbit |
Preparation of solid aluminium isopropoxide
I have recently duplicated the synthesis as described by Klute. I used 91% IPA. It was combined an ... |
25-5-2010 at 14:09
by: white rabbit |
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