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Phenyl Isocyanide: Not as bad as you may think! (Strange problem)
I made a similar product and also found the odor not that bad.
Phenylethyl isocyanide
Added scoo ... |
25-2-2024 at 09:44
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Boxwood odor
Not sure why no one looked at the literature for this compound, it is well known to be one of the mo ... |
9-1-2024 at 12:12
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Synthesis of thioacetone?
Have not found suitable location for thioacetone experiments, but have more than enough materials (k ... |
9-1-2024 at 10:51
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Acetone Acetal
Triacetone mannitol (mannitol acetone triketal)
Carried out according to Fischer https://doi.org/10 ... |
9-1-2024 at 10:44
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Synthesis of thioacetone?
Found a reference to stop selenoketone and telluroketone speculation. Instead of more odor, seems le ... |
14-8-2023 at 10:25
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Acetone Acetal
Dimethoxypropane (acetone dimethyl acetal)
110g acetone
120g methanol
1ml 30% HCl
40g MgSO4
Sti ... |
8-8-2023 at 18:41
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Acetone Acetal
Redistilled fraction 2 with aluminium foil insulated column. Pinch of sodium carbonate added to dist ... |
2-8-2023 at 04:35
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Synthesis of thioacetone?
During ketonic decarboxylation is there no free acid at all? Even so the high temperature will insta ... |
31-7-2023 at 06:55
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Synthesis of thioacetone?
If ketonic decarboxylation worked probably only get trithioacetone because of high temperature and a ... |
31-7-2023 at 05:12
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Acetone Acetal
Some patents say HCl works best because it has other effect not only catalyst. Could use HCl (aq) wi ... |
30-7-2023 at 12:40
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Synthesis of thioacetone?
Selenoketones dimerize, and telluroketones are very unstable so thioketones are easier to make.
T ... |
30-7-2023 at 12:28
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Acetone Acetal
No heat because it will cause the desiccant to release water. Should be complete reaction in 12h at ... |
29-7-2023 at 07:46
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Synthesis of thioacetone?
Found another acetal based procudure. Uses anhydrous ethanol instead of GAA and no hydroquinone.
... |
28-7-2023 at 04:39
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Acetone Acetal
Attempting to make acetone ethylene acetal (2,2-Dimethyl-1,3-dioxolane) to create thioacetone (proce ... |
28-7-2023 at 04:27
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aldol condensation of acetone on calcium carbide
Good tips Fery. Joints were not greased and acetone was leaking, next time will try teflon tape. For ... |
30-5-2023 at 05:03
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aldol condensation of acetone on calcium carbide
I attempted the acetone + CaOH -> DAA + iodine -> MO route.
200g unknown water content acet ... |
29-5-2023 at 20:55
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Synthesis of thioacetone?
Fery: Saw your synthesis of thioformaldehyde, very nice! Do you know how far you could smell the H2S ... |
17-1-2023 at 07:49
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Synthesis of thioacetone?
Both NileRed and LabCoatz did not follow the original procedure that produced the infamous odor. In ... |
16-1-2023 at 20:34
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