Originally posted by stoichiometric_steve
"The reaction was quenched by pouring into aq. ammonia (30 ml, 2M), resulting inorganic precipitate filtered off"
and thats where the reference is lacking quite some detail, because a pretty much unfilterable solid - Ti2O(OiPr)2 - is formed, which took ~1.5h for
vac. filtration of 500ml. Even the attempted filtration through a 2cm pad of celite didn't help much.
Would it maybe be helpful to make a slurry with celite and then filter through a celite pad? |