Originally posted by woelen
Thanks for your responses. It now is clear to me that simple distillation at 100..120 C of this compound is not wise. It will eat the glass and may
even lead to explosion. So, I should find some metal flask, in which to do the distillation, or use vacuum at lower temperature. I have no experience
yet with the latter, I'll first try with water at 60 C or so. I do have a vacuum pump (up to now I used it for other things only, such as filtering
and physics experiments). |