precursor - 14-12-2005 at 09:55
Hi!
Does anyone have any suggestions how to separate organ/water layers with constant cooling conditions?
Can I make some kind of setup with a regular separation funnel without too mouch trouble?
neutrino - 14-12-2005 at 14:22
Could you give some more background here? Your posts makes little sense in its present form.
precursor - 14-12-2005 at 16:49
My solution av organic product (an alkene) has a vere low boiling point, so I don't want it to evaporate in any step.
I'm sorry, my english is not too good, maybe it's hard to understand what I mean all the time.
edit; I've got an organic layer and a water layer, and I need to separate them, without any organic compound escaping... 
[Edited on 15-12-2005 by precursor]
DrP - 15-12-2005 at 03:23
Sounds like your on the right track with the seperating funnel. Keep it cool if your worried about evapouration - perhaps leave the lot in the
fridge for a bit before doing the seperation?
precursor - 15-12-2005 at 09:31
I'll stick to the fridge, I think... 