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Sciencemadness Discussion Board » Literature and Documentation » Prepublication » Benzotrichloride, Benzoyl Chloride, and Phthalyl Chloride - Illustrated Practical Guide Go To Bottom

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Author: Subject: Benzotrichloride, Benzoyl Chloride, and Phthalyl Chloride - Illustrated Practical Guide
slinky
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[*] posted on 23-10-2010 at 19:24
Awesome Write-up


I really enjoyed your post. Thanks :)
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Thor
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[*] posted on 6-7-2011 at 13:34


A great write up, really instructive. Planning to have a go soon myself, to obtain some acid chloride's. Can you recommend a light source to initiate the reaction? Would an array of UV LED's be sufficient, or does this require a high voltage metal vapour lamp or similar?
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Bestbmc
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[*] posted on 13-10-2021 at 16:40


I am looking to try this too, but I am unsure if I have the equipment. I have a 25w 254nm lamp, and it seems that it might be too low power, as it required 7 hours with a 1kw lamp. Has anyone had success with photo chlorinations with a low power bulb?

I looked for a more powerful lamp, but the only thing I found was reptile lamps, would it be worth it to buy a 100w reptile lamp?
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 Sciencemadness Discussion Board » Literature and Documentation » Prepublication » Benzotrichloride, Benzoyl Chloride, and Phthalyl Chloride - Illustrated Practical Guide   Go To Top