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TGSpecialist1
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Quote: Originally posted by karlos³  | I would love to see a reference for your imaginative tryptamine synthesis via hemetsberger.
Because that is something I am definitely not familiar with.
Its not that sensitive?
Just read the hyperlab report. |
Well yes, this procedure is just an idea that can be tried out but I don't see anything wrong or contradictory in it, all the parts make sense
separately and an experiment is the only way to know if it works together.
Unsuprisingly, the molecule becomes prone to decomposition once you put an azide group on it, which is done just before the thermal cyclisation step.
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karlos³
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Mood: oxazolidinic 8)
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Your dehydration is the most disturbing step to me personally, heating an azidoalcohol to 180°C 
To dehydrate it to a product, which has proven to be unstable even at freezing temperature!
Thats crazy.
Also, you wrote most of those reactions can be done one-pot?
How so?
But good luck if you're going to try this, I just hope for your safety, that you fail at something more harmless, before you get to this step or even
to the use of azides at all...
Because there is no chance this is going to work.
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