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[*] posted on 25-7-2010 at 20:15
how do these 2 chemicals react?


ok i hypothetically have Sodium nitrite (NaNO2) and Diethyl sulfate (C4H10SO4) and i want to make Nitroethane (C2H5NO2)

am i correct that 2 molecules of NaNO2 react with 1 molecule of C4H10SO4 to make 2 molecules of C2H5NO2?



[Edited on 26-7-2010 by lol]

[Edited on 26-7-2010 by lol]
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[*] posted on 25-7-2010 at 20:40


If you have to ask...


You shouldn't be using with diethyl sulfate, it's quite carcinogenic (believe me :-/ ). Nitroethane is also pretty flammable (like nitromethane).

My advice (after reading your other thread):

Find another line of work, preferably one that has no chemistry involved in it. Also, it might be beneficial to consider for a moment just what you may be getting yourself into...




Neither flask nor beaker.


"Kid, you don't even know just what you don't know. "
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[*] posted on 25-7-2010 at 21:03


thanx for pointing this hazard out, but this is just an example for educational purposes cause the recipe has all the numbers. i noticed this was a dangerous chemical so i'll use a different method with Sodium ethyl sulfate and Sodium nitrite. i also will be wearing a labcoat and protective glasses for the Nitroethane...what do you think about this model? labcoat ;)

[Edited on 26-7-2010 by lol]
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[*] posted on 26-7-2010 at 01:12


Quote:
Find another line of work,


Or hit the books like Chris Brown.




“If Edison had a needle to find in a haystack, he would proceed at once with the diligence of the bee to examine straw after straw until he found the object of his search.
I was a sorry witness of such doings, knowing that a little theory and calculation would have saved him ninety per cent of his labor.”
-Tesla
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[*] posted on 26-7-2010 at 03:39


Quote: Originally posted by lol  
the recipe has all the numbers






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[*] posted on 26-7-2010 at 09:28


lmao, im from holland

so how about these 2 chemicals? i dont got chemistry in school (cause they was tryina keep me dumb). i like to beleive 2 sodium nitrite and 1 diethyl sulfate make 2 nitroethane but the "recipe" says only half of the nitroethane will be produced

[Edited on 26-7-2010 by lol]
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[*] posted on 26-7-2010 at 09:31


So, which recipe amine are you trying to gas with HCl(g) and recrystallize, again?

[Edited on 26-7-2010 by peach]




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[*] posted on 26-7-2010 at 09:45


So you dropped out of school because they "was tryina keep" you dumb (and succeeded), and now you're mixing up carcinogens according to what you "like to beleive"?

This should end comically.
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[*] posted on 26-7-2010 at 09:46


Sodium ethyl sulfate and sodium nitrite can be distilled to give off nitro ethane, but you will also have an ethyl nitrite byproduct. You might want to use excess sodium ethyl sulfate to dilute the nitrite, otherwise you run the danger of exothermic oxidation/ explosion.
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[*] posted on 26-7-2010 at 12:31


Interesting point Hoveland, i will have to read up on that. Thanx!
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[*] posted on 26-7-2010 at 12:35


Quote: Originally posted by gardenvariety  
So you dropped out of school because they "was tryina keep" you dumb (and succeeded), and now you're mixing up carcinogens according to what you "like to beleive"?

This should end comically.


id be using a hazmat suit before i would mix these chemicals. im just trying to learn how it works (im not actually gonna brew this recipe)

[Edited on 26-7-2010 by lol]

[Edited on 26-7-2010 by lol]
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[*] posted on 26-7-2010 at 12:40


Quote: Originally posted by peach  
So, which recipe amine are you trying to gas with HCl(g) and recrystallize, again?

[Edited on 26-7-2010 by peach]

http://webcache.googleusercontent.com/search?q=cache:HgJxenX...

second 1
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[*] posted on 26-7-2010 at 13:05


lol,

don't do it yet. You will either kill or seriously injure yourself and yield will be too low anyway. Either order the nitroethane (very dangerous, not recommended!) go after phenethylamines (needs nitromethane which is available OTC) or try one of the "essential amphetamines". But stay clear of PM(M)A, these just suck.
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[*] posted on 26-7-2010 at 13:21


please elaborate on whats up with the phenethylamines and the essential amphetamines
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[*] posted on 26-7-2010 at 14:30


The relevant question is not how the chemicals react but how will you react
when exposed to them. Search this in google => "ethyl sulfate" MSDS

Competence in the practical application of procedures is directly proportional
to your ability to use search functions.

Enter the specific terms you cite into ' Advanced search ' in google as depicted
in the image attached below -

How to google.gif - 35kB

1 - Click ' Advanced search '

2 - Type in the search terms " inside quotation marks " if the term has more than a one word

3 - Restrict the search to the specific domain you posed your query.

doing the above will get you here _

http://www.google.com/search

4 - selecting ' cache ' highlights the relevent posts for you.

http://www.sciencemadness.org/talk/viewthread.php?tid=4711#p...
http://www.sciencemadness.org/talk/viewthread.php?tid=4711#p...

Another way
http://www.sciencemadness.org/talk/viewthread.php?tid=2995&a...

There are safer ways , see this PDF
http://www.sciencemadness.org/talk/files.php?pid=81599&a...

.
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[*] posted on 26-7-2010 at 14:58


ARRRRR, LAND LUBBARS ON ME QUARTAR DECK!



Quote:
please elaborate on whats up with the phenethylamines and the essential amphetamines


Phenethylamines & The essential ampethamines

Quote:
Competence in the practical application of procedures is directly proportional to your ability to use search functions.


BUW HA HA HAR, yar be correct. And yar can be google bashin' as yar say by makin' use o' the "trick" and knockin' out results with a -"trick". Thar be pages dedicated tar 'hacking' google searches to mine publicly available datar that often simply be not visible on the HTML front. For instance, yar be able to use it to download a lot o' free mp3's by enterin' search criteria that show up FTP file lists for those thar formats, sizes and names.

[Edited on 27-7-2010 by peach]




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[*] posted on 26-7-2010 at 16:29


y'all arent so helpfull as you might think you are :P

[Edited on 27-7-2010 by lol]

[Edited on 27-7-2010 by lol]
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[*] posted on 26-7-2010 at 16:39


Nitroethane synthesis has already been discussed in another thread, check that one out.

[Edited on 27-7-2010 by peach]




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[*] posted on 26-7-2010 at 18:12


Quote: Originally posted by lol  
y'all arent so helpfull as you might think you are :P


I get the feeling most of us were trying to be as unhelpful as possible.




“If Edison had a needle to find in a haystack, he would proceed at once with the diligence of the bee to examine straw after straw until he found the object of his search.
I was a sorry witness of such doings, knowing that a little theory and calculation would have saved him ninety per cent of his labor.”
-Tesla
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[*] posted on 26-7-2010 at 19:46


Quote: Originally posted by peach  
Nitroethane synthesis has already been discussed in another thread, check that one out.

[Edited on 27-7-2010 by peach]


ok maybe your right im gonna check it out

psychokinetic, i dont understand what you have against nitroethane
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[*] posted on 26-7-2010 at 22:42


Quote: Originally posted by lol  
please elaborate on whats up with the phenethylamines and the essential amphetamines

Step 1: Buy this book: http://transformpress.com/pihkal.html It's important that you buy the paperback version, not some ebook crap.
Step 2: Read it, ideally more than once
Step 3: Come back
This is kind of a bible for people interested in this kind of chemistry and not only the chemistry related comments are insightful.

PS: You might not realize it, but most people here are indeed quite helpful. The rest: http://www.penny-arcade.com/comic/2004/3/19/ - ignore them.
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[*] posted on 26-7-2010 at 22:58


Nitroethane? Hmmmmm. Do you mean Nitroethane, the DEA....list 1 precursor?

The difficult to obtain, and dangerous to produce material, that is the gateway to the easy synthesis of methamphetamine, and a plethora of psychotropic phenethylamines?

http://www.deadiversion.usdoj.gov/21cfr/cfr/1310/1310_02.htm...



[Edited on 27-7-2010 by zed]
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[*] posted on 26-7-2010 at 23:13


Quote: Originally posted by zed  
Nitroethane? Hmmmmm. Do you mean Nitroethane, the DEA....list 1 precursor?

The difficult to obtain, and dangerous to produce material, that is the gateway to the easy synthesis of methamphetamine, and a plethora of psychotropic phenethylamines?

Actually amphetamine, the common form in Europe, not methamphetamine. I doubt anyone would go to the length of N-methylating the resulting amphetamine.

I doubt the OP cares a lot about the DEA since he claims to be from the Netherlands. In any case, I would never order nitroethane with my real name. Especially not in the Netherlands with their domestic MDMA production.
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[*] posted on 26-7-2010 at 23:44


Turd,

You've never heard of using Nitroethane to produce Phenyl-2-Propanone, the classic Methamphetamine precursor?

In the era before the development of the P/I2 reduction of Ephedrine......Nitroethane was used to produce P2P. When severe restrictions were placed on Nitroethane, Benzaldehyde, and Methylamine...............Methamphetamine supply plummeted, and there was limited availability for many years.

At any rate "lol", when a new poster shows up, and starts innocently inquiring about Nitroethane.........The folks hereabouts laugh and roll their eyes.



[Edited on 27-7-2010 by zed]
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[*] posted on 27-7-2010 at 00:18


Actually no, I didn't realize that this used to be a common way of P2P manufacture. I hope you excuse my outside-of-US-centrism, but actually I don't care a lot how illicit drug production works in the US. I was under the impression that P2P was mostly made via phenylacetic acid. Of course I heard about the Nef reaction, but it always seemed extremely rude to me. It would break my heart to remove the nitrogen already in the right position. The more I think about it - what a waste of perfectly fine nitroethane. Plain old trivial P2P, what a joke. :(
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