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Author: Subject: Removal of superfine copper particles from stir bar
Draeger
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[*] posted on 1-7-2020 at 16:36
Removal of superfine copper particles from stir bar


Today I got some superfine copper particles stuck in the Teflon coating of the stir bar and it doesn't go off by a paper towel or scratching, and I have no nitric acid.

Is there any other way to remove them?




Collected elements:
Al, Cu, Ga, C (coal), S, Zn, Na

Collected compounds:

Inorganic:
NaOH; NaHCO3; MnCl2; MnCO3; CuSO4; FeSO4; aq. 30-33% HCl; aq. NaClO; aq. 9,5% ammonia; aq. 94-96% H2SO4; aq. 3% H2O2

Organic:
citric acid, sodium acetate, sodium citrate, petroleum, mineral oil
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Ubya
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[*] posted on 1-7-2020 at 16:41


Quote: Originally posted by Draeger  
Today I got some superfine copper particles stuck in the Teflon coating of the stir bar and it doesn't go off by a paper towel or scratching, and I have no nitric acid.

Is there any other way to remove them?


acetic acid + H2O2
HCl + H2O2
H2SO4 + H2O2

any acid and an oxidizer pretty much





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Draeger
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[*] posted on 1-7-2020 at 17:03


Quote: Originally posted by Ubya  
Quote: Originally posted by Draeger  
Today I got some superfine copper particles stuck in the Teflon coating of the stir bar and it doesn't go off by a paper towel or scratching, and I have no nitric acid.

Is there any other way to remove them?


acetic acid + H2O2
HCl + H2O2
H2SO4 + H2O2

any acid and an oxidizer pretty much

Oh wow, didn't think it'd be that easy. Thanks.

I know what the other two reaction products with H2O2 are, but what does acetic acid and H2O2 make?




Collected elements:
Al, Cu, Ga, C (coal), S, Zn, Na

Collected compounds:

Inorganic:
NaOH; NaHCO3; MnCl2; MnCO3; CuSO4; FeSO4; aq. 30-33% HCl; aq. NaClO; aq. 9,5% ammonia; aq. 94-96% H2SO4; aq. 3% H2O2

Organic:
citric acid, sodium acetate, sodium citrate, petroleum, mineral oil
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Syn the Sizer
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[*] posted on 1-7-2020 at 18:22


I believe it is just a solution of H2O2 and acetic acid. The H2O2 helps produce an oxide layer for the acid to attack.

[Edited on 2-7-2020 by Syn the Sizer]
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symboom
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[*] posted on 1-7-2020 at 22:27


Everyone is forgetting ammonia and air by shaking them in solution to make them soluble in ammonia as a complex nice and cheapest.

[Edited on 2-7-2020 by symboom]

[Edited on 2-7-2020 by symboom]
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