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solo
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Cyanuric Chloride : A useful reagent for converting carboxylic acids into chorides, esters, amides and peptides
K. Venkatamaran
Tet.Letters
32, 3037-3040 , 1979
Attachment: Cyanuric chloride - a useful reagent for converting carboxylic acids into chlorides, esters, amides and peptides.pdf (211kB) This file has been downloaded 246 times
It's better to die on your feet, than live on your knees....Emiliano Zapata.
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Monoamine
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So what's the source of the chlorides? Neither the cyanuric acid, the water, or the propionic acid have any. Surely you must be missing an ingredient.
(Edit) Just saw your post solo. So I guess you have to chlorinate the cyanuric acid first, which should not be too hard, because if you pluck a -OH
off while you look around for a Cl- to stick back on the molecule is nicely resonance stabilized. So just bathe the cyanuric acid in conc. HCl?
[Edited on 2-4-2022 by Monoamine]
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solo
International Hazard
Posts: 3975
Registered: 9-12-2002
Location: Estados Unidos de La Republica Mexicana
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Quote: Originally posted by Monoamine | So what's the source of the chlorides? Neither the cyanuric acid, the water, or the propionic acid have any. Surely you must be missing an ingredient.
(Edit) Just saw your post solo. So I guess you have to chlorinate the cyanuric acid first, which should not be too hard, because if you pluck a -OH
off while you look around for a Cl- to stick back on the molecule is nicely resonance stabilized. So just bathe the cyanuric acid in conc. HCl?
[Edited on 2-4-2022 by Monoamine] |
.....need to buy cyanuric chloride ...not sure that your theory of chlorination will work, but bears trying since cyanuric choride seems to be a bit
expensive....let me know if it works ....solo
It's better to die on your feet, than live on your knees....Emiliano Zapata.
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