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Author: Subject: How to make alloxan from murexide?
vano
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[*] posted on 7-9-2021 at 08:14
How to make alloxan from murexide?


Hi i found more than 50 years old murexide, but i think it's looks good. I want to make alloxan from murexide. What is best way? Does anyone have idea?



received_1807546019633951.jpeg - 188kB

[Edited on 7-9-2021 by vano]




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UC235
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[*] posted on 7-9-2021 at 17:48


Probably you could feed it into this prep: http://orgsyn.org/demo.aspx?prep=CV3P0037

With any luck, the NOx produced will destroy the imine nitrogen after hydrolysis
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vano
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[*] posted on 9-9-2021 at 09:19


Thanks! I will try



A narrow road cannot keep back Death, nor a rocky one; by him all are levelled, weak and strong-hearted; in the end the earth unites in one place youth and greybeard. Better a glorious death than shameful life!
—The Knight in the Panther's Skin
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