Peroksit
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PETN synthesis question
Hi
English is poor
What else I need to add in terms of security?
For Safety protective goggles , gloves , Runaway nitration for 2 litre cold water )
1) Nitration mixture cooled in the fridge (temperature: - or 0C .. 2 hours cooled)
2) Beaker the ice bath and Pentaerythritol it each time be scored as 1gram ( temperature temperature 5-7 degrees will not be allowed to rise )
3) Last Pentaeritritol is adding . 10 minutes later Nitration mixture hot water bath put 25 minutes After 25 minutes, poured into cold water ( hot
water bath 45 C )
4) Petn crystals wash with clear water . %1 sodium bicarbonate solition wash with petn crystals ( natural pH 7 pH is measured with pH paper )
5) PETN and Acetone is put in a glass container heated 50C ( hot water bath ) . PETN is After dissolving - PETN and acetone mixture poured cold water
> crystals appeared )
6) PETN is filtered . PETN wash with water >>> Drying
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hissingnoise
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There's a long thread on PETN, here!
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Peroksit
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Thanks man
my english is bad
I do not understand fully: S
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Peroksit
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Which method must i use for recrystallization? ( to purify/clean acid residue better )
using 2.5 ml acetone for each 1 gram petn ( pentaerythritol tetranitrate )
First Acetone and sodium bicarbonate had heated to 50 C.
Then petn ( pentaerythritol tetranitrate ) was added gradually to this mixture.
2-3 minutes later after petn ( pentaerythritol tetranitrate ) was dissolved entirely, mixture is pured to cold water.
at this stage ( this step ) which percent of sodium bicarbonate (gram) must i put into / (add to) acetone?
This method is correct??? İs there anything wrong? Is there anything I should add?
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Peroksit
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I have a question
PETN Do explodes during recrystallization? Do you?
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hyfalcon
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My god man, use the edit button instead of triple posting!
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