Sciencemadness Discussion Board
Not logged in [Login ]
Search the forums Search   Frequently Asked Questions FAQ   View member list Member List   Today's Posts Today's Posts   Forum Stats Stats Back to: sciencemadness.org
Sciencemadness Discussion Board » Fundamentals » Beginnings » Hydrazine generation in situ Go To Bottom

Printable Version  
Author: Subject: Hydrazine generation in situ
LeeBrown
Harmless
*



Posts: 3
Registered: 29-3-2013
Member Is Offline

Mood: No Mood

[*] posted on 30-9-2013 at 08:14
Hydrazine generation in situ

Hello, recently I found this patent with a procedure to synthesize 4,5-dichloro pyridazinone. In first example they reflux hydrazine hydrate with mucochloric acid in n-butanol. I wonder whether it is possible to use hydrazine chloride or sulfate with NaOH and generate hydrazine hydrate in situ. Any ideas are appreciated :)
View user's profile View All Posts By User
bfesser
Resident Wikipedian
 Thread Moved
30-9-2013 at 08:16
sonogashira
National Hazard
****



Posts: 555
Registered: 10-9-2006
Member Is Offline

Mood: No Mood

[*] posted on 30-9-2013 at 09:47


Sure. I've done a Wolff–Kishner reduction using hydrazine sulphate.
View user's profile View All Posts By User
LeeBrown
Harmless
*



Posts: 3
Registered: 29-3-2013
Member Is Offline

Mood: No Mood

[*] posted on 1-10-2013 at 06:15


But as far as I know neither hydrazine salts nor NaOH are soluble in butanol.
View user's profile View All Posts By User

 Sciencemadness Discussion Board » Fundamentals » Beginnings » Hydrazine generation in situ   Go To Top