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[*] posted on 8-11-2013 at 08:13
milk booster neutralization


Today i was trying to nitrate some milk powder exacted from milk with vinegar.
After nitration there was a staff that it looks like ETN but in had got a more yellow color.
For neutralization i used a saturated solution of water/sodium bicarbonate, and i deep into it the nitrated staff with a filter.
When neutralization stared, from slightly yellow the staff was, it starts to turn a really deep yellow color!! At the end, the hole staff it was disappeared and the solution turned to yellow.
When you are going to add some not nitrated milk powder into the above solution, nothing was happened, so i guess that the nitrated staff really can be destroyed by sodium bicarbonate.
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Gargamel
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[*] posted on 8-11-2013 at 13:43


Excuse my ignorance, but what is that supposed to be?
Lactose nitrate?
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Metacelsus
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[*] posted on 8-11-2013 at 13:59


WHY are you trying to nitrate milk powder? It seems like it would just produce non-energetic decomposition products (i.e. crap). Milk powder contains large amounts of fat and protein, which I doubt would nitrate well.





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[*] posted on 8-11-2013 at 14:44


Q: what is "staff?"



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[*] posted on 8-11-2013 at 15:42


He means stuff.



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[*] posted on 8-11-2013 at 16:22


If this is supposed to be lactose nitrate, it would be a good idea to try to first isolate lactose (Google that) then nitrate it according to patented procedures quoted, if I recall correctly, by Fedoroff in the Encyclopedia of Explosives and Related Items. Finally, check if the pure thing behaves with bicarbonate like the "milk booster".
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[*] posted on 8-11-2013 at 20:04


I think he is making Caesin nitrate. The Caesin is extracted from milk with vinegar then the extracted material is dried and nitrated. It is not that powerful though.I read up on it in one of them military manuals years ago but never attempted it myself. Seemed like too much hassle for a weak material.



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[*] posted on 8-11-2013 at 20:33


The fact that casein is a phosphoprotein probably explains the poor explosive power of its nitrated equivalent. If I remember correctly, nitrating protein usually just causes it to decompose, but can form a nitrated product if there are large amounts of aromatic amino acids.

https://en.wikipedia.org/wiki/Xanthoproteic_reaction




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[*] posted on 8-11-2013 at 22:10


It is said that this stuff it is really powerful, with VoD of 7.5-8 Km/s and it can be also used as a primary explosive. The reason i made that is to test its properties as a primary, and to see if it is can be used as a primary,
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[*] posted on 9-11-2013 at 05:26


i have read about this thing in one of those how to make primaries etc etc

anyhow i have seen a video with 120g of this stuff being setoff, it sure did go bang but it was not easy to compare..
i cant find the video now tho

no wait...
http://www.youtube.com/watch?v=_AVWJ8M7ke4

its not pure, and you cant tell if it would work on its own.. guess this might be the closest you will come to a test of this milk booster stuff?




~25 drops = 1mL @dH2O viscocity - STP
Truth is ever growing - but without context theres barely any such.

https://en.wikipedia.org/wiki/Solubility_table
http://www.trimen.pl/witek/calculators/stezenia.html
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[*] posted on 9-11-2013 at 05:27


You shouldnt be wasting your HNO3 on this, make some N2O5 out of it and you can totally be on another level.
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[*] posted on 9-11-2013 at 07:25


Quote: Originally posted by DubaiAmateurRocketry  
You shouldnt be wasting your HNO3 on this, make some N2O5 out of it and you can totally be on another level.


>HNO3
>make N2O5 out of it

HOW ? :o

yesterday i read at the Urbanski that HNO3 and H2SO4 will partially react to N2O4...but how the hell would someone make seperate N2O5 out of HNO3...

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[*] posted on 9-11-2013 at 08:41


Quote: Originally posted by VladimirLem  
Quote: Originally posted by DubaiAmateurRocketry  
You shouldnt be wasting your HNO3 on this, make some N2O5 out of it and you can totally be on another level.


>HNO3
>make N2O5 out of it

HOW ? :o

yesterday i read at the Urbanski that HNO3 and H2SO4 will partially react to N2O4...but how the hell would someone make seperate N2O5 out of HNO3...



P2O5 is sold in many chemical stores.
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[*] posted on 9-11-2013 at 10:43


Quote: Originally posted by DubaiAmateurRocketry  
Quote: Originally posted by VladimirLem  
Quote: Originally posted by DubaiAmateurRocketry  
You shouldnt be wasting your HNO3 on this, make some N2O5 out of it and you can totally be on another level.


>HNO3
>make N2O5 out of it

HOW ? :o

yesterday i read at the Urbanski that HNO3 and H2SO4 will partially react to N2O4...but how the hell would someone make seperate N2O5 out of HNO3...



P2O5 is sold in many chemical stores.


really^^...i dont think im able to buy this as an normal citizen (without getting trouble with the law)
your quote sounds like that its easy/possible to make N2O5 out of hno3:(
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[*] posted on 10-11-2013 at 06:37


i have considered SO3 for making +70% HNO3, but its very dangerous to handle..
P2O5 isnt controlled as phosphorus is however.. 250g for below 10 pounds at british ebay isnt that bad





~25 drops = 1mL @dH2O viscocity - STP
Truth is ever growing - but without context theres barely any such.

https://en.wikipedia.org/wiki/Solubility_table
http://www.trimen.pl/witek/calculators/stezenia.html
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[*] posted on 10-11-2013 at 10:54


Hi

i searched a lot for some sources to get phosphourus-containing dehydrating agents...

and i found that phosphoric acid will obtain when P2O3 reacts with H2O...

so, is it possible to dry/dehydrate phosphoric acid (seems to be a heavy reaction, wiki said) to get P2O3 ?

cause if i have P2O3 (already cool stuff) i could easiely react it with O2 to P2O5



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[*] posted on 15-11-2013 at 22:02


Use bicarbonate solution to neutralize and post your results about the power of milk booster . And there is already thready related to it
http://www.sciencemadness.org/talk/viewthread.php?tid=17030#...




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[*] posted on 16-11-2013 at 00:21


I had already used sodium bicarbonate for neutralization as you can see the description on of my first post.

Also i have seen the thread you post about that, but it has not something about that we discuss here
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[*] posted on 17-11-2013 at 05:40


Sorry didn't read ur post completely just try to wash it with water a lot of time and try to detonate it and post ur results



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[*] posted on 17-11-2013 at 08:29


Yea, when i will try it, i will post my results.
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[*] posted on 17-11-2013 at 09:56


Quote: Originally posted by underground  
Yea, when i will try it, i will post my results.


Take care and do in small scales.

Take some basic protection also, so we dont repeat tragedy like this one
http://www.sciencemadness.org/talk/viewthread.php?tid=22554
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[*] posted on 17-11-2013 at 13:43


Quote: Originally posted by DubaiAmateurRocketry  
Quote: Originally posted by underground  
Yea, when i will try it, i will post my results.


Take care and do in small scales.

Take some basic protection also, so we dont repeat tragedy like this one
http://www.sciencemadness.org/talk/viewthread.php?tid=22554


Yea, that is true
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