HardAsSteel
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Where to buy a 50 Liter Magnetic Hotplate Stirrer?
I do essential Oil distillation under vacuum and can not find any
50 Liter Magnetic Hotplate Stirrer , attention HOTPLATE magnetic stirrer.
they are always limited to 20 Liter.
there are normal Magnetic Stirrers for big volumes but always without hotplate.
where can I buy a 50 Liter Magnetic Hotplate Stirrer in europe?
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Elemental Phosphorus
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You could buy a 50 liter heating mantle, and put it on top of a 50 liter magnetic stirrer. You said you already found a stirrer, here is a listing for
a 50 liter mantle:
For a steam distillation at that scale, I would recommend a fabricated metal still, a motorized mechanical stirrer, and a oil or sand bath for
heating. If you get a metal still, then you could also heat by direct flame.
http://www.neobits.com/ace_glass_12050_41_50l_low_pro_mantle...
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HardAsSteel
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this would be a vacuum distillation, I can not find any air tight overhead stirrers which fit on my vessle for the vaccum distillation
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Praxichys
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Why stir a vacuum distillation when you could just use an ebulliator? Pull a very thin tip on piece of glass tube (probably 3 of them for 50L) and
keep them submerged in the liquid and the other end open to the atmosphere. The vacuum will pull air through the tube at a very slow rate (assuming
you made the tip small enough) and prevent bumping.
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HardAsSteel
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[Edited on 8-5-2017 by HardAsSteel]
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lab-equip
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You are going to use a big rare metal magnetic stirbar!
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PirateDocBrown
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Quote: Originally posted by Praxichys  | Why stir a vacuum distillation when you could just use an ebulliator? Pull a very thin tip on piece of glass tube (probably 3 of them for 50L) and
keep them submerged in the liquid and the other end open to the atmosphere. The vacuum will pull air through the tube at a very slow rate (assuming
you made the tip small enough) and prevent bumping.
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Yes, exactly! I have had good results just using a Pasteur pipette. And the clamp is used to control the gas flow. This can easily be used with an
inert gas, if needed.
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BILLBUILDS
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www.alibaba.com
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