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Author: Subject: 5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Etanol
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[*] posted on 14-8-2024 at 21:28


The experiment showed that an excess of ascorbic acid at pH <3.5 reduces Cu(++) in solution to a metallic copper in a few hours at room temperature or in 3-5 minutes in a hot solution.
At PH>3.5, Cu(OH)2 is formed, that is instantly reduced with ascorbic acid to copper (I) oxide Cu2O at room temperature.
How to avoid these impurities in DBX-1 synthesis?

[Edited on 15-8-2024 by Etanol]
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